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Perkin 1 Abstracts: Solid Phase Organic Synthesis John Christopher Catherine McCusker Susan Booth and Jason Tierney pg 1-vii; DOI: 10.1039/a909287a |
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Synthesis of heterocycles by radical cyclisation W. Russell Bowman Colin F. Bridge and Philip Brookes pg 1; DOI: 10.1039/a808141g |
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Nickel(0)-catalyzed asymmetric cross-coupling reactions of allylic compounds with arylboronic acids Kang-Go Chung Yoshihiro Miyake and Sakae Uemura pg 15; DOI: 10.1039/a908076g |
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Fmoc/Acyl protecting groups in the synthesis of polyamide (peptide) nucleic acid monomers Zoltán Timár Lajos Kovács Györgyi Kovács and Zoltán Schmél pg 19; DOI: 10.1039/a907832k |
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Two ring transformations of 3-methyl-5-nitropyrimidin-4(3H)-one for the construction of azaheterocycles Nagatoshi Nishiwaki Tomoko Adachi Kengo Matsuo Hui-Ping Wang Tomoko Matsunaga Yasuo Tohda and Masahiro Ariga pg 27; DOI: 10.1039/a907728f |
Novel xanthine oxidase inhibitor studies. Part 3. Convenient and general syntheses of 3-substituted 7H-pyrazolo[4,3-e]-1,2,4-triazolo[4,3-c]pyrimidin-5(6H )-ones as a new class of potential xanthine oxidase inhibitorsTomohisa Nagamatsu Takayuki Fujita and Kazuki Endo pg 33; DOI: 10.1039/a907673e |
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Three approaches to the synthesis of L-leucine selectively labelled with carbon-13 or deuterium in either diastereotopic methyl group Matthew D. Fletcher John R. Harding Rachael A. Hughes Nicholas M. Kelly Holger Schmalz Andrew Sutherland and Christine L. Willis pg 43; DOI: 10.1039/a907598d |
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A simple synthetic method for chiral 1,2-epoxides and the total synthesis of a chiral pheromone epoxide Zhi-Bo Zhang Zhi-Min Wang Yu-Xiu Wang Huan-Quan Liu Gui-Xin Lei and Min Shi pg 53; DOI: 10.1039/a907396e |
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An efficient semisynthesis of 7-deoxypaclitaxel from taxine Radomir N. Sai  i and Radomir Matovi pg 59; DOI: 10.1039/a907288h |
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Bi–KOH. An efficient reagent for the coupling of nitroarenes to azo and azoxy compounds Dhrubojyoti Dey Laskar Dipak Prajapati and Jagir S. Sandhu pg 67; DOI: 10.1039/a907287j |
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Lipase promoted asymmetric trans-esterification of 4-alkyl-, 3-alkyl- and 3,4-dialkyloxetan-2-ones with ring-opening Naoko Sakai Satoru Ageishi Hiroshi Isobe Yoshiyuki Hayashi and Yukio Yamamoto pg 71; DOI: 10.1039/a907220i |
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Diastereoselective addition reactions of racemic chiral vinyl sulfimides Charlotte P. Rayner (née Baird) Andrew J. Clark Stuart M. Rooke Tim J. Sparey and Paul C. Taylor pg 79; DOI: 10.1039/a907064h |
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Studies on pyrazines. Part 37. Synthesis of 6-propionylpteridine-2,4(1H,3H)-dione and its 1- and/or 3-methyl derivatives from marine natural products Nobuhiro Sato and Shunsuke Fukuya pg 89; DOI: 10.1039/a906572e |
Baker s yeast mediated enantioselective synthesis of the bisabolene sesquiterpenes (+)-epijuvabione and (–)-juvabioneClaudio Fuganti and Stefano Serra pg 97; DOI: 10.1039/a905977f |
Synthesis and reactions of  -fluorovinylphosphonium saltsTakeshi Hanamoto Keiko Shindo Miki Matsuoka Yasuhide Kiguchi and Michio Kondo pg 103; DOI: 10.1039/a905878h |
Issue 2
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Perkin 1 Abstracts: Natural Product Synthesis Robert Narquizian and Jens Kaufmann pg 2-vii; DOI: 10.1039/a909283h |
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Applications of stoichiometric organotransition metal complexes in organic synthesis Alex C. Comely Susan E. Gibson (née Thomas) and Surojit Sur pg 109; DOI: 10.1039/a903026c |
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Imines, enamines and oximes Joseph P. Adams pg 125; DOI: 10.1039/a808142e |
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The strategy for Co2(CO)8-catalyzed double carbonylative [2+2+1] cycloaddition or [2+2+2] cycloaddition reaction of triynes: a new synthetic method for tetracyclic compounds Seung Uk Son Se-Jung Paik Sang Ick Lee and Young Keun Chung pg 141; DOI: 10.1039/a909605a |
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A reductive amination of carbonyls with amines using decaborane in methanol Jong Woo Bae Seung Hwan Lee Young Jin Cho and Cheol Min Yoon pg 145; DOI: 10.1039/a909506c |
An unusual observation in the rhodium carbenoids: [1,4]-migration in the sugar-derived -diazo- -ketoestersVijaya N. Desai Nabendu N. Saha and Dilip D. Dhavale pg 147; DOI: 10.1039/a908453c |
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Concerning the synthesis and enantioselective rearrangements of episulfoxides Alexander J. Blake Paul A. Cooke Jackie D. Kendall Nigel S. Simpkins and Susan M. Westaway pg 153; DOI: 10.1039/a908391j |
Some observations relating to the use of 1-aryl-4-alkoxypiperidin-4-yl groups for the protection of the 2 -hydroxy functions in the chemical synthesis of oligoribonucleotidesWayne Lloyd Colin B. Reese Quanlai Song Anthony M. Vandersteen Cristina Visintin and Pei-Zhou Zhang pg 165; DOI: 10.1039/a908149f |
Synthesis and evaluation of  -borono--amino acids as active-site probes of arginase and nitric oxide synthasesSylvain Collet François Carreaux Jean-Luc Boucher Stéphanie Pethe Michel Lepoivre Renée Danion-Bougot and Daniel Danion pg 177; DOI: 10.1039/a908140b |
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Regioselectivity in lignin biosynthesis. The influence of dimerization and cross-coupling Kaisa Syrjänen and Gösta Brunow pg 183; DOI: 10.1039/a907919j |
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Synthesis of sesquiterpene allylic alcohols and sesquiterpene dienes from Cupressus bakeri and Chamaecyparis obtusa Koon-Sin Ngo and Geoffrey D. Brown pg 189; DOI: 10.1039/a907752i |
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Stereoselective [2+2+2] cocyclotrimerization of oxa- and azabenzonorbornadienes with alkynes catalyzed by nickel complexes: first transition metal-mediated synthesis of isobenzofuran and isoindole precursors Thota Sambaiah Daw-Jen Huang and Chien-Hong Cheng pg 195; DOI: 10.1039/a907654i |
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Reactions of some N-(2,5-dimethoxyaryl)thiobenzamides: en route to an analogue of kuanoniamine A Yvette A. Jackson Michael A. Lyon Norman Townsend Kettyna Bellabe and Fernando Soltanik pg 205; DOI: 10.1039/a907633f |
Reductive decomplexation of  -allyltricarbonyliron lactone complexes: a new route to stereodefined acyclic 1,5-diols and 1,5,7-triolsSteven V. Ley Svenja Burckhardt Liam R. Cox and Julia M. Worrall pg 211; DOI: 10.1039/a907630a |
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Efficient synthesis of protected -phenylethylamines, enantiomerically pure protected -phenyl--benzylethylamines and -phenyl--isopropylethylamines using organozinc chemistry Christopher Hunter Richard F. W. Jackson and Harshad K. Rami pg 219; DOI: 10.1039/a907629h |
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Synthesis of haptens and their protein conjugates for immunological determination of nitrate esters and nitramines G. Michael Blackburn Ian G. Beadham Harry Adams Alistair P. Hutchinson and Stephen Nicklin pg 225; DOI: 10.1039/a906884h |
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1,3-Dipolar cycloaddition of azomethine ylides derived from imines and difluorocarbene to alkynes: a new active Pb-mediated approach to 2-fluoropyrrole derivatives Mikhail S. Novikov Alexander F. Khlebnikov Elena S. Sidorina and Rafael R. Kostikov pg 231; DOI: 10.1039/a905518e |
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The synthesis and conformational aspects of a novel dioxopiperazine—a possible -turn constraint John S. Davies Malgosia Stelmach-Diddams Regis Fromentin Alun Howells and Ron Cotton pg 239; DOI: 10.1039/a904943f |
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Radical cyclization of highly functionalized precursors: stereocontrol of ring closure of acyclic 1-substituted-2,4-dihydroxylated hex-5-enyl radicals Arlène Roland Thierry Durand David Egron Jean-Pierre Vidal and Jean-Claude Rossi pg 245; DOI: 10.1039/a904206g |
Issue 3
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Perkin 1 Abstracts: Solid Phase Organic Synthesis John Christopher Catherine McCusker Susan Booth and Jason Tierney pg 3-ix; DOI: 10.1039/b000127i |
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Construction of (Z,Z) skipped 1,4-dienes. Application to the synthesis of polyunsaturated fatty acids and derivatives Sandrine Durand Jean-Luc Parrain and Maurice Santelli pg 253; DOI: 10.1039/a907643c |
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Catalytic asymmetric processes Heather Tye pg 275; DOI: 10.1039/a900861f |
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A versatile synthetic route to quinoxaline, pyrazine and 1,2,4-triazine substituted -amino acids from vicinal tricarbonyls Robert M. Adlington Jack E. Baldwin David Catterick and Gareth J. Pritchard pg 299; DOI: 10.1039/a909722h |
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The synthesis of novel heterocyclic substituted -amino acids; further exploitation of -amino acid alkynyl ketones Robert M. Adlington Jack E. Baldwin David Catterick Gareth J. Pritchard and Lam T. Tang pg 303; DOI: 10.1039/a909720a |
Biotransformations of benzoylacetonitrile with the fungus Curvularia lunata: highly diastereo- and enantioselective synthesis of -alkyl -hydroxy nitriles and  -amino alcoholsVicente Gotor Juan R. Dehli and Francisca Rebolledo pg 307; DOI: 10.1039/a909721j |
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Reductive amination of carboxylic acids and [11C]magnesium halide carboxylates Cécile Perrio-Huard Catherine Aubert and Marie-Claire Lasne pg 311; DOI: 10.1039/a908991h |
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Reductive thioalkylation of a pyranonaphthoquinone Margaret A. Brimble and Michael R. Nairn pg 317; DOI: 10.1039/a908680c |
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Structure and biosynthesis of kendomycin, a carbocyclic ansa-compound from Streptomyces Helge B. Bode and Axel Zeeck pg 323; DOI: 10.1039/a908387a |
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-Chloronitroso compounds derived from carbohydrate ketones: cycloadditions with cyclic dienes, a synthesis of (–)-physoperuvine and a formal synthesis of (+)-epibatidine Adrian Hall Patrick D. Bailey David C. Rees Georgina M. Rosair and Richard H. Wightman pg 329; DOI: 10.1039/a908333b |
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Formation of medium-size bridged ring systems via ring-closing metathesis of 2,5-disubstituted-2,3-dihydro-1H-pyrroles Samantha J. Bamford Kees Goubitz Hester L. van Lingen Tim Luker Henk Schenk and Henk Hiemstra pg 345; DOI: 10.1039/a908272g |
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A simple synthesis of (+)- and (–)-alkaloid 241D and C-4 epimers Stéphane Ciblat Pierre Calinaud Jean-Louis Canet and Yves Troin pg 353; DOI: 10.1039/a908265d |
A variety of products from a  simple reaction of [1-(6-acetyl-2-naphthyl)piperidin-4-yl]methyl 4-methylbenzenesulfonate with nucleophiles in DMF–K2CO3Simon  eh and Andrej Petri pg 359; DOI: 10.1039/a908243c |
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First application of triflic acid for selective cleavage of glycosidic linkages in structural studies of a bacterial polysaccharide from Pseudoalteromonas sp. KMM 634 Andrei V. Perepelov Sof ya N. Senchenkova Aleksander S. Shashkov Nadezhda A. Komandrova Svetlana V. Tomshich Lyudmila S. Shevchenko Yuriy A. Knirel and Nikolay K. Kochetkov pg 363; DOI: 10.1039/a908141k |
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Kinetic resolution of primary 2-methyl-substituted alcohols viaPseudomonas cepacia lipase-catalysed enantioselective acylation Ove Nordin Ba-Vu Nguyen Carin Vörde Erik Hedenström and Hans-Erik Högberg pg 367; DOI: 10.1039/a908023f |
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Rhenium catalysed epoxidations with hydrogen peroxide: tertiary arsines as effective cocatalysts Michiel C. A. van Vliet Isabel W. C. E. Arends and Roger A. Sheldon pg 377; DOI: 10.1039/a907975k |
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Enantiopure N-protected -amino glyoxals Paul Darkins Michelle Groarke M. Anthony McKervey Hazel M. Moncrieff Noreen McCarthy and Mark Nieuwenhuyzen pg 381; DOI: 10.1039/a907948c |
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Synthesis of novel hypotensive aromatic thiocarbamate glycosides Rubeena Saleem and Jerrold Meinwald pg 391; DOI: 10.1039/a907050h |
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Stereoselective formation of 1,2-diiodoalkenes and their application in the stereoselective synthesis of highly functionalised alkenes via Suzuki and Stille coupling reactions Nadine Hénaff and Andrew Whiting pg 395; DOI: 10.1039/a906832e |
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Mesoions and ketene valence isomers. Pyrrolo[1,2-a]pyridinylium olates and (2-pyridyl)carbonylketenes Xuan Ye John Andraos Hervé Bibas Ming Wah Wong and Curt Wentrup pg 401; DOI: 10.1039/a906831g |
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Re-investigation of optical sensing properties of boronic-acid-appended ReI complexes for saccharides Toshihisa Mizuno Takayuki Fukumatsu Masayuki Takeuchi and Seiji Shinkai pg 407; DOI: 10.1039/a906708f |
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Effects of methylene chains on photoreactions of diphenylalkanediones and phenylalkenones Mitsunobu Nakamura Masamichi Miki and Tetsuro Majima pg 415; DOI: 10.1039/a906631d |
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The synthesis of novel bisphosphonates as inhibitors of phosphoglycerate kinase (3-PGK) Neil A. Caplan Christopher I. Pogson David J. Hayes and G. Michael Blackburn pg 421; DOI: 10.1039/a906507e |
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Ring opening reactions of 2-trialkylsilylaziridines Alan R. Bassindale Patricia A. Kyle Marie-Claire Soobramanien and Peter G. Taylor pg 439; DOI: 10.1039/a906233e |
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Further unexpected boron trifluoride-catalyzed reactions of taxoids with - and -4,20-epoxides Hirokazu Hosoyama Hideyuki Shigemori and Jun ichi Kobayashi pg 449; DOI: 10.1039/a905799d |
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Synthesis and circular dichroism of steroids with 2,3-dihydro-1-benzofuran and 4H-benzopyran chromophores; revision of the absolute configuration of some norneolignans from Krameria cystisoides Tibor Kurtán Eszter Baitz-Gács Zsuzsa Majer and Sándor Antus pg 453; DOI: 10.1039/a905697a |
Square pegs in round holes. Preparation and intramolecular complexation of cubyl substituted -cyclodextrins and of an adamantane analogueBruce L. May Philip Clements John Tsanaktsidis Christopher J. Easton and Stephen F. Lincoln pg 463; DOI: 10.1039/a905390e |
Issue 4
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Perkin 1 Abstracts: Natural Product Synthesis Robert Narquizian pg 4-xi; DOI: 10.1039/b000126k |
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Sodium perborate and sodium percarbonate: further applications in organic synthesis Alexander McKillop and William R. Sanderson pg 471; DOI: 10.1039/a804579h |
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Novel methods for the synthesis of three-, four-, five-, six- and seven-membered, saturated and partially unsaturated carbocycles Richard C. Hartley and Stuart T. Caldwell pg 477; DOI: 10.1039/a804421j |
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Reductive amination of aromatic aldehydes and ketones with nickel boride Ira Saxena Ruli Borah and Jadab C. Sarma pg 503; DOI: 10.1039/a909770h |
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Synthesis of new water-soluble phosphonium salts and their Wittig reactions in water Matthew G. Russell and Stuart Warren pg 505; DOI: 10.1039/a909495d |
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Asymmetric -substitution versus aza Diels–Alder reaction of electron deficient N-sulfonyl imines Paul E. Morgan Ray McCague and Andrew Whiting pg 515; DOI: 10.1039/a909116e |
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New routes to 5-substituted oxazoles Matthew S. Addie and Richard J. K. Taylor pg 527; DOI: 10.1039/a908987j |
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Stereochemical control in the synthesis of tetrahydrofurans by cyclisation of diols with [1,2]-phenylsulfanyl migration Varinder K. Aggarwal Jason Eames María-Jesús Villa Sara McIntyre Francis H. Sansbury and Stuart Warren pg 533; DOI: 10.1039/a908810e |
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Regiochemistry in aryl radical cyclisations (5-exoversus 6-endo) of N-vinylic 2-iodobenzamides Hiroyuki Ishibashi Kohei Ohata Michiyo Niihara Tatsunori Sato and Masazumi Ikeda pg 547; DOI: 10.1039/a908678a |
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Imidazoquinolinethiones from 8-aminoquinolines by a novel peri-participation Thierry Besson Charles W. Rees David G. Roe and Valérie Thiéry pg 555; DOI: 10.1039/a908952g |
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Rapid synthesis of 2-cyanobenzothiazole, isothiocyanate and cyanoformanilide derivatives of dapsone Thierry Besson Jérôme Guillard and Charles W. Rees pg 563; DOI: 10.1039/a908742g |
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The first isolation and crystal structure of a boron difluoro complex (isoflavone yellow). Biologically active intermediates produced during isoflavone synthesis Sreenivasan Balasubramanian Donald L. Ward and Muraleedharan G. Nair pg 567; DOI: 10.1039/a908915b |
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A straightforward preparation of primary alkyl triflates and their utility in the synthesis of derivatives of ethidium Steven A. Ross Marguerite Pitié and Bernard Meunier pg 571; DOI: 10.1039/a908389h |
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New copper(I) and iron(II) complexes for atom transfer radical macrocyclisation reactions Floryan De Campo Dominique Lastécouères and Jean-Baptiste Verlhac pg 575; DOI: 10.1039/a908245j |
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A new and efficient synthesis of ortho- and para-benzoquinones of cardanol derivatives by the catalytic system MeReO3–H2O2 Raffaele Saladino Veronica Neri Enrico Mincione Stefano Marini Massimiliano Coletta Chiara Fiorucci and Paolino Filippone pg 581; DOI: 10.1039/a908073b |
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The synthesis of 2-arylmethyl-6-hydroxybenzenecarbonitriles from the base-mediated aryne reaction of bromophenols with arylacetonitriles Sagun Tandel Hongming Zhang Nabil Qadri George P. Ford and Edward R. Biehl pg 587; DOI: 10.1039/a907980g |
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Synthesis of alkyldibenzophosphole 5-oxides Ernesto Durán Dolores Velasco and Francisco López-Calahorra pg 591; DOI: 10.1039/a907399j |
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First preparation and characterization of the allenic carotenoids (all-E,6S)- and (9Z,6S)-neoxanthin Aase Strand and Synnøve Liaaen-Jensen pg 595; DOI: 10.1039/a907366c |
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Synthesis of novel unsymmetrical squarylium dyes absorbing in the near-infrared region Shigeyuki Yagi Yutaka Hyodo Shinya Matsumoto Naoki Takahashi Hiroshi Kono and Hiroyuki Nakazumi pg 599; DOI: 10.1039/a907335c |
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Bis-porphyrin arrays. Part 2. The synthesis of asymmetrically substituted bis-porphyrins Richard Beavington and Paul L. Burn pg 605; DOI: 10.1039/a907059a |
Issue 5
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Perkin 1 Abstracts: Solid Phase Organic Synthesis John Christopher Catherine McCusker Susan Booth and Jason Tierney pg 5-xi; DOI: 10.1039/b000731p |
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Preparative biotransformations Stanley M. Roberts pg 611; DOI: 10.1039/a908303k |
A new cycloheptenone annulation method: use of the bifunctional reagent (Z )-5-iodo-1-tributylstannylpent-1-ene in organic synthesisEdward Piers Shawn D. Walker and Ralph Armbrust pg 635; DOI: 10.1039/a909922k |
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Microwave accelerated selective and facile deprotection of allyl esters catalyzed by Montmorillonite K-10 Anil S. Gajare Nadim S. Shaikh Bhushan K. Bonde and Vishnu H. Deshpande pg 639; DOI: 10.1039/a909265j |
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Vinyl isonitriles in radical cascade reactions: formation of cyclopenta-fused pyridines and pyrazines Isabelle Lenoir and Marie L. Smith pg 641; DOI: 10.1039/a908630g |
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On the preparation of some phospholipid analogues Judith E. Browne Richard T. Freeman Jeremy C. Russell and Peter G. Sammes pg 645; DOI: 10.1039/a910266n |
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Preparation of phospholipid analogues using the phosphoramidite route Judith E. Browne Michael J. Driver Jeremy C. Russell and Peter G. Sammes pg 653; DOI: 10.1039/a910270l |
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Synthesis of 3-substituted isofagomine analogues using an unusual syn hydrogenation reaction Anders Lohse Henrik H. Jensen Peter Bach and Mikael Bols pg 659; DOI: 10.1039/a908340e |
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Synthesis of 3-C-hydroxymethyl- and 3-deoxyisofagomine and investigation of their binding to -glucosidase Henrik H. Jensen Anders Lohse Bent O. Petersen Jens Ø. Duus and Mikael Bols pg 667; DOI: 10.1039/a909869k |
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Atom transfer radical cyclisations of activated and unactivated N-allylhaloacetamides and N-homoallylhaloacetamides using chiral and non-chiral copper complexes Andrew J. Clark Floryan De Campo Robert J. Deeth Robert P. Filik Sylvain Gatard Nicola A. Hunt Dominique Lastécouères Gerard H. Thomas Jean-Baptiste Verlhac and Hathaichanuk Wongtap pg 671; DOI: 10.1039/a909666c |
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Samarium(II)-mediated 4-exo-trig cyclisations of unsaturated aldehydes. A stereoselective approach to functionalised cyclobutanols Derek Johnston Catherine F. McCusker Kenneth Muir and David J. Procter pg 681; DOI: 10.1039/a909549g |
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A titanium naphtholate approach for the synthesis of analogues of griseusin A Margaret A. Brimble Michael R. Nairn and Josephine S. O. Park pg 697; DOI: 10.1039/a909243i |
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Stereospecific conversion of (1R*,3S*)- and (1R*,3R*)-3-cyclohexyl-1-phenylpropane-1,3-diol into the corresponding 2,4-disubstituted oxetanes Tajassus Aftab Christabel Carter Martin Christlieb Jennifer Hart and Adam Nelson pg 711; DOI: 10.1039/a909163g |
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Preparation and NMR studies of 3-selenaheptadecanoic and 4-selenaoctadecanoic acid, RSe(CH2)nC(O)OH (R=C14H29, n=1 and 2), and their methyl esters Khaled I. Doudin Rolf K. Berge Nils Åge Frøystein and Jon Songstad pg 723; DOI: 10.1039/a909142d |
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Asymmetric synthesis of 3-angeloyloxy-4-hydroxyeudesman-8-one, purported sesquiterpene from Pluchea quitoc Estela Muri Alice Kanazawa Eliezer Barreiro and Andrew E. Greene pg 731; DOI: 10.1039/a909112b |
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Studies on synthesis of optically active twelve-membered diynes: a convergent construction of a twelve-membered diketodiyne compound with C2 symmetry Chisato Mukai Eiji Kasamatsu Takao Ohyama and Miyoji Hanaoka pg 737; DOI: 10.1039/a909089d |
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Secondary mould metabolites. Part 58. Modifications in basic conditions and Michael additions of the protoilludane sesquiterpene tsugicoline A; some implications for the biogenesis of other sesquiterpenoids produced by Basidiomycetes Alberto Arnone Cristiana De Gregorio Andrea Mele Gianluca Nasini and Orso Vajna de Pava pg 745; DOI: 10.1039/a908912h |
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Carbohydrate -oxoketene N,O-ketals in the synthesis of dihydroquinolines Götz Scheffler Francois Montavon Michael Hennig and Hans Peter Wessel pg 753; DOI: 10.1039/a908806g |
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The synthesis of 3-methyleneindol-2(3H)-ones related to mitomycins via 5-exo-dig aryl radical cyclisation Shirley A. Brunton and Keith Jones pg 763; DOI: 10.1039/a907920c |
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Intramolecular organolithium addition to indol-2(3H)-ones; an approach to the synthesis of pyrrolo[1,2-a]indoles and pyrido[1,2-a]indoles Keith Jones and John M. D. Storey pg 769; DOI: 10.1039/a909548i |
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A highly regio- and stereoselective synthesis of (Z)-3-arylidene-2,3-dihydro-5H-1,4-benzodioxepin-5-ones and (Z)-3-arylidene-1,2,3,5-tetrahydro-4,1-benzoxazepin-5-ones through palladium–copper catalysis Gopeswar Chaudhuri and Nitya G. Kundu pg 775; DOI: 10.1039/a908682j |
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Synthesis of 2-(substituted methyl)quinolin-8-ols and their complexation with Sn(II) Chitoshi Kitamura Naoyuki Maeda Noboru Kamada Mikio Ouchi and Akio Yoneda pg 781; DOI: 10.1039/a908636f |
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A novel method for the synthesis of substituted naphthalenes and phenanthrenes Charles B. de Koning Joseph P. Michael and Amanda L. Rousseau pg 787; DOI: 10.1039/a908361h |
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Syntheses of isochromane analogues of the michellamines and korupensamines Charles B. de Koning Joseph P. Michael and Willem A. L. van Otterlo pg 799; DOI: 10.1039/a908367g |
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Novel glucocorticoid antedrugs possessing a C16,17-fused -lactone ring Keith Biggadike Sean M. Lynn Panayiotis A. Procopiou the late Rupert E. Shaw and Christopher Williamson pg 813; DOI: 10.1039/a908358h |
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Synthesis and chemical reactivity of thiophenoxyphenylalanine bioisosteres, suitable synthons for the design of HIV protease inhibitors G. Priem L. Rocheblave C. De Michelis J. Courcambeck and J. L. Kraus pg 819; DOI: 10.1039/a907483j |
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A facile preparation of indium enolates and their Reformatsky- and Darzens-type reactions Tsunehisa Hirashita Kenji Kinoshita Hatsuo Yamamura Masao Kawai and Shuki Araki pg 825; DOI: 10.1039/a907334e |
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A new approach to the synthesis of nucleosides of 1,2,4-triazole El Sayed H. El Ashry Laila F. Awad and Martin Winkler pg 829; DOI: 10.1039/a904200h |
Issue 6
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Perkin 1 Abstracts: Natural Product Synthesis Robert Narquizian and Jacqueline Milne pg 6-xi; DOI: 10.1039/b000732n |
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Professor Gerald Pattenden pg 6-ix; DOI: 10.1039/b001289k |
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The synthesis of thiols, selenols, sulfides, selenides, sulfoxides, selenoxides, sulfones and selenones David J. Procter pg 835; DOI: 10.1039/a901128e |
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A novel photochromism of biindenylidene in crystal form Koichi Tanaka and Fumio Toda pg 873; DOI: 10.1039/a910194m |
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Total syntheses and re-assignment of configurations of the cyclopeptides lissoclinamide 4 and lissoclinamide 5 from Lissoclinum patella Christopher D. J. Boden and Gerald Pattenden pg 875; DOI: 10.1039/a909360e |
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Total synthesis and assignment of configuration of the thiazoline-based cyclopeptide cyclodidemnamide isolated from the sea squirt Didemnum molle Christopher D. J. Boden Mark Norley and Gerald Pattenden pg 883; DOI: 10.1039/a909363j |
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The first chemical synthesis of UDP--D-galactofuranose Yury E. Tsvetkov and Andrei V. Nikolaev pg 889; DOI: 10.1039/b000210k |
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Asymmetric synthesis of the northern segment of ephedradine C Michael G. N. Russell Raymond Baker Richard G. Ball Steven R. Thomas Nancy N. Tsou and José L. Castro pg 893; DOI: 10.1039/a909816j |
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Synthesis and enzyme-catalysed reductions of 2-oxo acids with oxygen containing side-chains Gurdip Bhalay Sarah Clough Lee McLaren Andrew Sutherland and Christine L. Willis pg 901; DOI: 10.1039/a909677i |
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Synthesis of ()-isofagomine and its stereoisomers from arecoline Steen Uldall Hansen and Mikael Bols pg 911; DOI: 10.1039/a909472e |
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Reactions of selenothioic acid S-esters with trivalent phosphorus compounds: new synthetic methods for -phosphoryl alkyl sulfides and alkyl selenides Toshiaki Murai Chiyoko Izumi Toshihide Itoh and Shinzi Kato pg 917; DOI: 10.1039/a909469e |
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Synthesis of a novel tweezers-type host aiming at chiral discrimination by circular dichroism spectroscopy Shigeyuki Yagi Hirokazu Kitayama and Toru Takagishi pg 925; DOI: 10.1039/a909468g |
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Interaction of novel cationic meso-tetraphenylporphyrins in the ground and excited states with DNA and nucleotides Pavel Kubát Kamil Lang Pavel Anzenbacher Jr. Karolina Jursíková Vladimír Král and Benjamin Ehrenberg pg 933; DOI: 10.1039/a909466k |
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Synthesis of (+)-(1R,2R,4R,6S)-1,6-epoxy-4-benzyloxycyclohexan-2-ol, a key precursor to inositol monophosphatase inhibitors, from (–)-quinic acid Jürgen Schulz Martin W. Beaton and David Gani pg 943; DOI: 10.1039/a909292g |
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Towards peptide isostere libraries: aqueous aldol reactions on hydrophilic solid supports Anette Graven Morten Grøtli and Morten Meldal pg 955; DOI: 10.1039/a909246c |
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Synthesis and evaluation of D-glucosamine-selective fluorescent sensors Christopher R. Cooper and Tony D. James pg 963; DOI: 10.1039/a909145i |
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Heterocyclic free radicals. Part 1. 4,5-Diazafluorene derivatives of Koelschs free radical: an EPR and metal-ion complexation study M. John Plater Steven Kemp and Eric Lattmann pg 971; DOI: 10.1039/a909109b |
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Syntheses of polycyclic compounds by oxidative coupling of azulene-1-azoarenes Alexandru C. Razus pg 981; DOI: 10.1039/a907402c |
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Oxidative benzylic substitution of azulene-1-azo(4-methylbenzene)s Alexandru C. Razus and Carmen Nitu pg 989; DOI: 10.1039/a908862h |
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Synthesis and X-ray structure of stable 2H-isoindoles Takashi Murashima Ryuji Tamai Keiji Nishi Kentaroh Nomura Ken-ichi Fujita Hidemitsu Uno and Noboru Ono pg 995; DOI: 10.1039/a908641b |
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Clay catalyzed conversion of isatoic anhydride to 2-(o-aminophenyl)oxazolines Anil S. Gajare Nadim S. Shaikh Gowda K. Jnaneshwara Vishnu H. Deshpande Thottappilli Ravindranathan and Ashutosh V. Bedekar pg 999; DOI: 10.1039/a908564e |
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Synthesis and structure–activity studies of 8- and 9-analogues of 14,17-ethanoestradiol James R. Bull and Pieter D. de Koning pg 1003; DOI: 10.1039/a908375h |
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Thermal reaction of diastereomeric benzocyclobutenols. Evidence for reversible opening of 1,2-dihydrobenzocyclobutenols to hydroxy-o-xylylenes Etsuya Kawata Masaichi Saito and Michikazu Yoshioka pg 1015; DOI: 10.1039/a908326j |
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Synthesis and binding properties of a macrobicyclic receptor for N-protected peptides with a carboxylic acid terminus Peter D. Henley Christopher P. Waymark Iain Gillies and Jeremy D. Kilburn pg 1021; DOI: 10.1039/a908090b |
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Palladium(II)-mediated 11C-carbonylative coupling of diaryliodonium salts with organostannanes—a new, mild and rapid synthesis of aryl [11C]ketones Mohammed H. Al-Qahtani and Victor W. Pike pg 1033; DOI: 10.1039/a907803g |
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Heterocalixarenes Part 3: Bis-oxo-bridged calix[1]cyclicurea[3]arene and calix[1]cyclicurea[1]pyridine[2]arenes. Synthesis, X-ray crystal structure and conformational analysis Subodh Kumar Dharam Paul Geeta Hundal Maninder Singh Hundal and Harjit Singh pg 1037; DOI: 10.1039/a906883j |
Issue 7
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Perkin 1 Abstracts: Solid Phase Organic Synthesis John Christopher Catherine McCusker Fiona McKerlie Tanya Wildman Jason Tierney and Bernard Wathey pg 7-vii; DOI: 10.1039/b001752n |
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Recent developments in indole ring synthesis—methodology and applications Gordon W. Gribble pg 1045; DOI: 10.1039/a909834h |
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Tandem peroxidase–glucose oxidase catalysed enantioselective sulfoxidation of thioanisoles Krzysztof Okrasa Eryka Guibé-Jampel and Michel Therisod pg 1077; DOI: 10.1039/b000529k |
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Chemistry of 4-dicyanomethylene-1,2,6-thiadiazines Panayiotis A. Koutentis and Charles W. Rees pg 1081; DOI: 10.1039/b000964o |
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Reaction of tetracyanoethylene with SCl2; new molecular rearrangements Panayiotis A. Koutentis and Charles W. Rees pg 1089; DOI: 10.1039/b000209g |
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The reaction of - and -methylenelactams with nitrones. Influence of electronic and geometric factors on the stereoselectivity of their 1,3-dipolar cycloaddition Séverinne Rigolet Jean Marie Mélot Joel Vébrel Angèle Chiaroni and Claude Riche pg 1095; DOI: 10.1039/b000129p |
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Synthesis of perfluoroalkylated sugars catalyzed by rabbit muscle aldolase (RAMA) Wei Zhu and Zuyi Li pg 1105; DOI: 10.1039/a910336h |
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Organolithium addition to styrene and styrene derivatives: scope and limitations Xudong Wei Paul Johnson and Richard J. K. Taylor pg 1109; DOI: 10.1039/a910195k |
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Base catalysed rearrangement of N-alkyl-O-acyl hydroxamic acids: synthesis of 2-acyloxyamides Andrew J. Clark Yassair S. S. Al-Faiyz Michael J. Broadhurst Divya Patel and Joanne L. Peacock pg 1117; DOI: 10.1039/a909903d |
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Palladium catalysed formal 6-endo-trig approaches to pumiliotoxin alkaloids: interception of the elusive cyclopropyl intermediate Stephanie Feutren Helena McAlonan David Montgomery and Paul J. Stevenson pg 1129; DOI: 10.1039/a909774k |
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Reactions of triene-conjugated diazo-compounds: reaction paths from o-(1,3-dienyl)aryldiazomethanes to 3,8-methano-1,2-diazocines and to pyrrolo[2,1-a]phthalazines via intramolecular (3+2) and 1,1-cycloaddition reactions John T. Sharp Paul Wilson Simon Parsons and Robert O. Gould pg 1139; DOI: 10.1039/a909516k |
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Photocycloaddition of arylethenes to 2-substituted-1,4-naphthoquinones and reactions of the cyclobutane adduct isomers Stephanie Cleridou Christopher Covell Anita Gadhia Andrew Gilbert and Patcharawalai Kamonnawin pg 1149; DOI: 10.1039/a909384b |
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Short practical synthesis of (3R,4R,5R,6R)-tetrahydroxyazepane and (3S,4S,5S,6S)-tetrahydroxyazepane from D- and L-chiro-inositol, respectively Gavin F. Painter and Andrew Falshaw pg 1157; DOI: 10.1039/a908986a |
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A conjugate from a laminin-related peptide, Tyr-Ile-Gly-Ser-Arg, and chitosan: efficient and regioselective conjugation and significant inhibitory activity against experimental cancer metastasis, Yasuhiro Nishiyama Tomoko Yoshikawa Nobumichi Ohara Keisuke Kurita Keiko Hojo Haruhiko Kamada Yasuo Tsutsumi Tadanori Mayumi and Koichi Kawasaki pg 1161; DOI: 10.1039/a908145c |
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Single-bead structure elucidation. Requirements for analysis of combinatorial solid-phase libraries by Nanoprobe MAS-NMR spectroscopy Charlotte H. Gotfredsen Morten Grøtli Marianne Willert Morten Meldal and Jens Ø Duus pg 1167; DOI: 10.1039/a906835j |
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The synthesis of 2-trialkylsilylaziridines from vinyltrialkylsilanes or the reaction of -chloro--silyl carbanions with imines Alan R. Bassindale Patricia A. Kyle Marie-Claire Soobramanien and Peter G. Taylor pg 1173; DOI: 10.1039/a905182a |
Issue 8
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Perkin 1 Abstracts: Natural Product Synthesis Robert Narquizian and Jacqueline Milne pg 8-vii; DOI: 10.1039/b001753l |
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A comparative study of the reduction by ascorbate of 1,1,3,3-tetraethylisoindolin-2-yloxyl and of 1,1,3,3-tetramethylisoindolin-2-yloxyl Lucien Marx Robert Chiarelli Thierry Guiberteau and André Rassat pg 1181; DOI: 10.1039/b001891k |
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Synthesis of a newly isolated APJ receptor peptide ligand using recombinant DNA technology and chemical cleavage reactions Masato Suenaga Takashi Itoh Masanori Miwa Nobuyuki Koyama Shuji Hinuma Chieko Kitada Osamu Nishimura and Masahiko Fujino pg 1183; DOI: 10.1039/b000152j |
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Initiation of radical cyclisation reactions using dimanganese decacarbonyl. A flexible approach to preparing 5-membered rings Bruce C. Gilbert Wilhelm Kalz Chris I. Lindsay P. Terry McGrail Andrew F. Parsons and David T. E. Whittaker pg 1187; DOI: 10.1039/b000835o |
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Hydrogenphosphonate synthesis of sugar phosphomonoesters Dmitry V. Yashunsky and Andrei V. Nikolaev pg 1195; DOI: 10.1039/b000727g |
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Bridged (-alkoxyalkyl)CoIII(salen) complexes by intramolecular alkoxycobaltation of unactivated alkenes: new models for coenzyme B12 Rolf Blaauw Irene E. Kingma Jan H. Laan Juul L. van der Baan Sijbe Balt Martinus W. G. de Bolster Gerhard W. Klumpp Wilberth J. J. Smeets and Anthony L. Spek pg 1199; DOI: 10.1039/b000196l |
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Efficient solid-phase synthesis of regioregular head-to-tail-coupled oligo(3-alkylthiophene)s up to a dodecamer Thomas Kirschbaum Christoph A. Briehn and Peter Bäuerle pg 1211; DOI: 10.1039/b000123f |
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Syntheses and pKa determination of 1-(o-hydroxyphenyl)imidazole carboxylic esters James P. Collman Zhong Wang Min Zhong and Li Zeng pg 1217; DOI: 10.1039/b000119h |
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Algal carotenoids. Part 64. Structure and chemistry of 4-keto-19-hexanoyloxyfucoxanthin with a novel carotenoid end group Einar Skarstad Egeland José Luis Garrido Manuel Zapata Miguel Angel Maestro and Synnøve Liaaen-Jensen pg 1223; DOI: 10.1039/a910345g |
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Bis-porphyrin arrays. Part 3.The synthesis of model bis-porphyrin dimers and an electrochemical study Richard Beavington and Paul L. Burn pg 1231; DOI: 10.1039/a910323f |
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The reaction of 3-nitropyridine with sulfite ions; a pathway to 2,5-disubstituted pyridines Jan M. Bakke Eli Ranes Christian Rømming and Ingrid Sletvold pg 1241; DOI: 10.1039/a909875e |
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Substituted 3,4-pyridynes: clean cycloadditions Stephen J. Connon and Anthony F. Hegarty pg 1245; DOI: 10.1039/a909772d |
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Intramolecular complexation in modified -cyclodextrins: a preparative, nuclear magnetic resonance and pH titration study Michael J. Field Bruce L. May Philip Clements John Tsanaktsidis Christopher J. Easton and Stephen F. Lincoln pg 1251; DOI: 10.1039/a909766j |
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Direct methoxylation of nitroarenes and nitroazaarenes with alkaline methoxides via nucleophilic displacement of an aromatic hydrogen atom Takehiko Kawakami and Hitomi Suzuki pg 1259; DOI: 10.1039/a909675b |
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Alkylating properties of synthetic trioxanes related to artemisinin Jérôme Cazelles Boris Camuzat-Dedenis Olivier Provot Anne Robert Joëlle Mayrargue and Bernard Meunier pg 1265; DOI: 10.1039/a909408c |
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Preparation of chiral -monofluoroalkylphosphonic acids and their evaluation as inhibitors of protein tyrosine phosphatase 1B Christopher C. Kotoris Wendy Wen Alan Lough and Scott D. Taylor pg 1271; DOI: 10.1039/a908086d |
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13C Labelling and electrospray mass spectrometry reveal a de novo route for inositol biosynthesis in Leishmania donovani parasite Parmeshwari Sahai Mamta Chawla and Ram A. Vishwakarma pg 1283; DOI: 10.1039/b000262n |
Issue 9
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Perkin 1 Abstracts: Solid Phase Organic Synthesis John Christopher Catherine McCusker Fiona McKerlie Tanya Wildman Jason Tierney and Bernard Wathey pg 9-xi; DOI: 10.1039/b002651o |
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Saturated oxygen heterocycles Mark C. Elliott pg 1291; DOI: 10.1039/a903885j |
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Exploitation of ylide steric bulk to alter cyclopropanation outcome during the reaction of 1,2-dioxines and stabilised phosphorus ylides Thomas D. Avery Ben W. Greatrex Dennis K. Taylor and Edward R. T. Tiekink pg 1319; DOI: 10.1039/b001975p |
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The first practical approach to optically pure cyclopropanes derived from trans-hydroxy enones Francine N. Palmer and Dennis K. Taylor pg 1323; DOI: 10.1039/b001973i |
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A highly efficient synthesis of L--2-deoxy-4-thio-1-purine nucleosides as potential antiviral agents Hea Ok Kim Lak Shin Jeong Sun Nan Lee Soo Jeong Yoo Hyung Ryong Moon Kil Soo Kim and Moon Woo Chun pg 1327; DOI: 10.1039/b001240h |
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Application of Baylis–Hillman methodology in a chemoselective synthesis of 3-acyl-2H-1-chromenes Perry T. Kaye and Xolani W. Nocanda pg 1331; DOI: 10.1039/b001148g |
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Synthesis of a novel peptide, galanin-like peptide (GALP), by a combination of recombinant DNA technology and chemical cleavage reactions Takashi Itoh Masanori Miwa Masato Suenaga Tetsuya Ohtaki Chieko Kitada Osamu Nishimura and Masahiko Fujino pg 1333; DOI: 10.1039/b001087l |
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A convergent synthesis of heterocyclic dendrimers using the 1,3-dipolar cycloaddition reaction of organic azides and acetylenedicarboxylate esters Grete Van Wuytswinkel Bert Verheyde Frans Compernolle Suzanne Toppet and Wim Dehaen pg 1337; DOI: 10.1039/b000025f |
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Enantiopure synthesis of carbohydrates mediated by oxyselenenylation of 3,4-dihydro-2H-pyran Kwan Soo Kim Choong Woon Moon Jong Il Park and Se-Hee Han pg 1341; DOI: 10.1039/a910166g |
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Enantioselective toluene dioxygenase catalysed di- and tri-hydroxylation of monosubstituted benzenes Derek R. Boyd Narain D. Sharma Nigel I. Bowers John Duffy John S. Harrison and Howard Dalton pg 1345; DOI: 10.1039/b000753f |
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Atroposelective attack of nucleophiles and electrophiles on 2-acyl-1-naphthamides and their enolates Jonathan Clayden Neil Westlund Roy L. Beddoes and Madeleine Helliwell pg 1351; DOI: 10.1039/b000668h |
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Atroposelective attack of nucleophiles on 2-formyl-1-naphthamides and their derivatives: chelation and non-chelation control Jonathan Clayden Catherine McCarthy Neil Westlund and Christopher S. Frampton pg 1363; DOI: 10.1039/b000669f |
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Atropisomeric diastereoisomers from nucleophilic attack on 8-acyl-1-naphthamides Jonathan Clayden Neil Westlund and Christopher S. Frampton pg 1379; DOI: 10.1039/b000670j |
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Furo[3,4-b]benzofurans: synthesis and reactions Tim Traulsen and Willy Friedrichsen pg 1387; DOI: 10.1039/b000619j |
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A formal synthesis of reserpine: hydrindane approach to the Woodwards ring-E precursor Goverdhan Mehta and D. Srinivasa Reddy pg 1399; DOI: 10.1039/b000430h |
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Experiments related to the synthesis and analysis of a hydrazine library Ulf Ragnarsson Bengt Fransson and Leif Grehn pg 1405; DOI: 10.1039/b000139m |
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Synthesis of a fluorescent derivative of 6-N-[N-(6-aminohexyl)carbamoyl)-2,3-dideoxyadenosine 5-triphosphate for detection of nucleic acids Thomas Schoetzau Sven Klingel Regina Wartbichler Ulrich Koert and Joachim W. Engels pg 1411; DOI: 10.1039/b000120l |
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Unexpected regioselectivity in nitration of 3-aminoquinoxalin-2(1H)-ones Csaba Gönczi Éva Csikós Benjamin Podányi Tamás Nusser Zsolt Böcskei and István Hermecz pg 1417; DOI: 10.1039/a910234p |
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The suitability of anion-accelerated oxy-Cope rearrangement as a probe to study -facial selectivity. An experimental study with (6-methyl-1-oxa-4-thiaspiro[4.5]dec-6-en-7-yl)(allyl)methanols Veejendra K. Yadav Duraiswamy A. Jeyaraj and Masood Parvez pg 1423; DOI: 10.1039/a909839i |
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Bis[2-(2-pyridyl)phenyl] diselenide, a more effective catalyst for oxidation of alcohols to carbonyl compounds Hitoshi Ehara Masato Noguchi Shinsei Sayama and Tetsuo Onami pg 1429; DOI: 10.1039/a909819d |
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Unusual reactivity of cis-2-benzoyl-1-benzyl-3-phenylaziridine with P-nucleophiles—ring opening vs. the Abramov reaction Andrzej E. Wróblewski Waldemar Maniukiewicz and Wies  awa Karolczak pg 1433; DOI: 10.1039/a909521g |
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Hajos–Parrish ketone: approaches toward C-ring precursors of 7-deoxytaxol Marja Lajunen and Ari Koskinen pg 1439; DOI: 10.1039/a909471g |
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Synthesis of a group of diosgenyl saponins with combined use of glycosyl trichloroacetimidate and thioglycoside donors Hai Yu Biao Yu Xiangyang Wu Yongzheng Hui and Xiuwen Han pg 1445; DOI: 10.1039/a909218h |
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Synthesis and solid-state polymerization of 5-(2-methylthio-4-methylpyrimidin-5-yl)penta-2,4-diyn-1-ol and of several of its derivatives Jiang-Hong Wang Yu-Quan Shen Cong-Xuan Yu and Jing-Hai Si pg 1455; DOI: 10.1039/a908958f |
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A new methodology for the synthesis of -amino acids Mukund P. Sibi and Prasad K. Deshpande pg 1461; DOI: 10.1039/a908747h |
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A novel thiopyran-4-thione synthesis and crystal structure of a thiopyran-4-thione Jan Oskar Jeppesen Niels Thorup and Jan Becher pg 1467; DOI: 10.1039/a908068f |
Issue 10
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Perkin 1 Abstracts: Natural Product Synthesis Robert Narquizian and Jacqueline Milne pg 10-ix; DOI: 10.1039/b001652m |
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Recent advances in the construction of -D-mannose and -D-mannosamine linkages Jonathan J. Gridley and Helen M. I. Osborn pg 1471; DOI: 10.1039/a909165c |
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Nickel catalyzed cascade conversion of propargyl halide and propargyl alcohol into 4,6-dimethyl-5-cyano-2-pyrone in water Noé Rosas Manuel Salmon Pankaj Sharma Cecilio Alvarez Rodrigo Ramirez José-Luis Garcia and Henri Arzoumanian pg 1493; DOI: 10.1039/b002338h |
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A new reaction of arylphospholes: site-selective phosphorylation through reaction with phosphorus tribromide György Keglevich Tungalag Chuluunbaatar András Dobó and László Tke pg 1495; DOI: 10.1039/b002042g |
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Convergent synthesis and preliminary biological evaluation of ()-B-norrhazinal Martin Banwell Alison Edwards Jason Smith Ernest Hamel and Pascal Verdier-Pinard pg 1497; DOI: 10.1039/b001731k |
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Catalytic hydrogen-transfer reactions of benzylic and allylic alcohols with palladium compounds in the presence of vinyl acetate or under an ethylene atmosphere Masahiko Hayashi Kanako Yamada and Shu-zo Nakayama pg 1501; DOI: 10.1039/b001385o |
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Synthesis of four possible stereoisomers of 1,2-epoxy-3-hydroxyerythrinans: total synthesis of an alkenoid-type erythrinan alkaloid, ()-erythratidine Shinzo Hosoi Motoyoshi Nagao Yoshisuke Tsuda Kimiaki Isobe Takehiro Sano and Tomihisa Ohta pg 1505; DOI: 10.1039/b001906m |
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Synthesis of N-propionylated (S)-(–)-2-(pyrrolidin-2-yl)propan-2-ol and its use as a chiral auxiliary and selectivity marker in asymmetric aldol reactions Erik Hedenström Fredrik Andersson and Mats Hjalmarsson pg 1513; DOI: 10.1039/b001730m |
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The synthesis of stable 1,3,4-triphenylphospholes Tuula-A Niemi Paul L. Coe and Stephen J. Till pg 1519; DOI: 10.1039/b000692k |
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Reactions of tetrafluoroethene oligomers. Part 15. Reactions of perfluoro-3,4-dimethylhex-3-en-2-one; a highly reactive ,-unsaturated ketone Paul L. Coe Ian R. Owen and Stephen J. Till pg 1529; DOI: 10.1039/b001263g |
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Reactions of tetrafluoroethene oligomers. Part 16. The synthesis and reactions of perfluoro[2,3-dimethyl-2-(3-methylpentan-3-yl)]-2H-azirine: a source of 2,3-bis(trifluoromethyl)aziridine derivatives Paul L. Coe and Michael I. Cook pg 1537; DOI: 10.1039/b001456g |
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On the development of NAD(P)H-sensitive fluorescent probes Nicola L. Maidwell M. Reza Rezai Carl A. Roeschlaub and Peter G. Sammes pg 1541; DOI: 10.1039/b001296n |
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Lewis acid-induced rearrangment of -[bis(methylthio)methylene]ethyl-2-styrylcyclopropylcarbinols: unexpected formation of a novel bicyclo[3.2.1]octadiene framework U. K. Syam Kumar Pranab K. Patra Hiriyakkanavar Ila Hiriyakkanavar Junjappa and Parimal K. Bharadwaj pg 1547; DOI: 10.1039/b001043j |
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Efficient regio- and diastereo-controlled synthesis of 1,1- and 1,1,2,2-functionalised ferrocenes and the formation of 2-oxa[3]ferrocenophanes Michael A. Carroll Andrew J. P. White David A. Widdowson and David J. Williams pg 1551; DOI: 10.1039/b000833h |
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Catalytic tin radical mediated tricyclisations. Part 1. Monocyclisation studies David R. Kelly and Mark R. Picton pg 1559; DOI: 10.1039/b000661k |
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Catalytic tin radical mediated tricyclisations. Part 2 David R. Kelly and Mark R. Picton pg 1571; DOI: 10.1039/b000662i |
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On reduction of ,-unstaurated ketones and the respective allylic alcohols, bearing a phenylsulfonyl or phenylsulfanyl group in the position. Hydroxy group-controlled stereoselective reduction of 3- and 3-hydroxy-4-(phenylsulfonyl)cholest-4-ene Karol Michalak Wiaczes aw Stepanenko and Jerzy Wicha pg 1587; DOI: 10.1039/b000600i |
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Enantioselective conversion of meso-cyclic disulfides to chiral cyclic sulfides via desulfurization with chiral aminophosphines Yoshihiro Miyake Hiroya Takada Kouichi Ohe and Sakae Uemura pg 1595; DOI: 10.1039/b000191k |
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Leaving group effects in reductively triggered fragmentation of 4-nitrobenzyl carbamates Bridget M. Sykes Michael P. Hay Dubravka Bohinc-Herceg Nuala A. Helsby Charmian J. O Connor and William A. Denny pg 1601; DOI: 10.1039/b000135j |
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A novel Suzuki-type cross-coupling reaction of cyclopropylboronic esters with benzyl bromides Han Chen and Min-Zhi Deng pg 1609; DOI: 10.1039/b000121j |
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Synthesis of trovafloxacin using various (1,5,6)-3-azabicyclo[3.1.0]hexane derivatives Timothy Norris Tamim F. Braish Michael Butters Keith M. DeVries Joel M. Hawkins Stephen S. Massett Peter R. Rose Dinos Santafianos and Constantine Sklavounos pg 1615; DOI: 10.1039/a910340f |
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Free radical chemistry. Part 10. Addition of acyclic and cyclic alkanes to hexafluoropropene Richard D. Chambers Robert W. Fuss Robert C. H. Spink Martin P. Greenhall Alan M. Kenwright Andrei S. Batsanov and Judith A. K. Howard pg 1623; DOI: 10.1039/a909777e |
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Free radical chemistry. Part 11. Additions of cyclic and acyclic alcohols and diols to hexafluoropropene Richard D. Chambers Patrick Diter Stephen N. Dunn Christopher Farren Graham Sandford Andrei S. Batsanov and Judith A. K. Howard pg 1639; DOI: 10.1039/a909778c |
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The synthesis of vicinal halohydrin phosphates via highly regioselective ring opening of epoxides with dialkyl halophosphate Yixiang Ding and Jun Hu pg 1651; DOI: 10.1039/a909613b |
Issue 11
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Professor Varinder K. Aggarwal pg 11-iv; DOI: 10.1039/b001932l |
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Perkin 1 Abstracts: Solid Phase Organic Synthesis John Christopher Catherine McCusker Fiona McKerlie Tanya Wildman Jason Tierney and Bernard Wathey pg 11-xi; DOI: 10.1039/b003114n |
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Cobalt mediated cyclisations Anthony J. Fletcher and Steven D. R. Christie pg 1657; DOI: 10.1039/a903168e |
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Toluene dioxygenase-mediated oxidation of aromatic substrates with remote chiral centers Vu Bui Trond Vidar Hansen Yngve Stenstrøm Douglas W. Ribbons and Tomas Hudlicky pg 1669; DOI: 10.1039/b002143l |
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The synthesis of novel trisphosphoranylphosphine and its oxide Wenhu Wang Ruzhen Cao and Lunzu Liu pg 1673; DOI: 10.1039/b001917h |
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1,7-Asymmetric induction of chirality in a Mukaiyama aldol reaction using -allyltricarbonyliron lactone complexes: highly diastereoselective synthesis of -substituted -hydroxy carbonyl compounds Steven V. Ley and Edward A. Wright pg 1677; DOI: 10.1039/b002056g |
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Dipolarophilic behaviour of (arylsulfonyl)allenes towards nitrilimines Gianluigi Broggini and Giorgio Molteni pg 1685; DOI: 10.1039/b001947j |
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Stereoselectivity in the synthesis of conformationally constrained vicinally dihydroxylated cyclic -amino acids Kristin Hammer Jing Wang Mette Lene Falck-Pedersen Christian Rømming and Kjell Undheim pg 1691; DOI: 10.1039/b001779p |
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Stereo and chemical course of acid-catalyzed double bond migration of cholesta-5,7-dien-3-ol to 5-cholesta-8,14-dien-3-ol Hideharu Seto Shozo Fujioka Hiroyuki Koshino Suguru Takatsuto and Shigeo Yoshida pg 1697; DOI: 10.1039/b001726o |
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A versatile and convenient method for the synthesis of substituted benzo[a]carbazoles and pyrido[2,3-a]carbazoles Charles B. de Koning Joseph P. Michael and Amanda L. Rousseau pg 1705; DOI: 10.1039/b001685n |
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Approaches to the synthesis of non-racemic 3-substituted isoindolinone derivatives Steven M. Allin Christopher J. Northfield Michael I. Page and Alexandra M. Z. Slawin pg 1715; DOI: 10.1039/b001569p |
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Selective C-acylation of CH-active dicarbonyl compounds with ketenylidenetriphenylphosphorane: syntheses and structures of 3-phosphoranylideneacyltetronic acids, 3-phosphoranylideneacyl-4-oxocoumarins, and 4-phosphoranylideneacylpyrazol-5-ones Rainer Schobert Sven Siegfried Mark Nieuwenhuyzen Wolfgang Milius and Frank Hampel pg 1723; DOI: 10.1039/b001541p |
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Pyrolysis reactions of nonafluorobiphenyl-4-yl prop-2-enyl ether: a remarkable rearrangement reaction of an intramolecular Diels–Alder product Andrei S. Batsanov Gerald M. Brooke Darren Holling and Alan M. Kenwright pg 1731; DOI: 10.1039/b001356k |
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Heteroaromatic ethers of phenols in nickel-catalysed ipso-replacement reactions with magnesium, zinc and tin organometallic compounds Amadeu F. Brigas and Robert A. W. Johnstone pg 1735; DOI: 10.1039/b001333l |
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Hydroxy-substituted triarylcarbenium bromides. Synthesis, structure, derivatization and facile conversion to highly substituted xanthenes Maarten B. Dinger and Michael J. Scott pg 1741; DOI: 10.1039/b001032o |
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High valence vanadium complex promoted selective rearrangement of epoxides to aldehydes or ketones Fernando Martínez Carmen del Campo and Emilio F. Llama pg 1749; DOI: 10.1039/b000965m |
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Regio- and stereo-selectivity issues in radical brominations of allylic units of vinylogous esters/carbonates bearing the 2,3,4,6-tetra-O-acetyl--D-glucopyranosyl auxiliary and in nucleophilic displacements of the derived allylic bromides A. Paula Esteves Ana M. Freitas Clive M. Raynor and Richard J. Stoodley pg 1753; DOI: 10.1039/b000901f |
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Chemoenzymatic synthesis of the non-tricyclic antidepressants Fluoxetine, Tomoxetine and Nisoxetine Hui-Ling Liu Bård Helge Hoff and Thorleif Anthonsen pg 1767; DOI: 10.1039/b000846j |
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[2+2] Cycloaddition of cyclic vinyl phosphonates with ketenes Suzanne M. Ruder and Min Ding pg 1771; DOI: 10.1039/b000014k |
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One-pot synthesis of oligomeric aryl-substituted PPV analogs with extended -conjugation Ben-Ami Feit and Ludmila Buzhansky pg 1777; DOI: 10.1039/a905710b |
Issue 12
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Perkin 1 Abstracts: Natural Product Synthesis Robert Narquizian Jacqueline Milne and Duncan McAurthur pg 12-ix; DOI: 10.1039/b003116j |
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The control of remote asymmetric centres via reduction of acyclic carbonyl functions Helen Sailes and Andrew Whiting pg 1785; DOI: 10.1039/b000155o |
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Enantioselective total synthesis of heliannuols D and A Kenya Takabatake Izumi Nishi Mitsuru Shindo and Kozo Shishido pg 1807; DOI: 10.1039/b003553j |
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New preparative routes to isosorbide 5-mononitrate Chris Brown Richard W. Marston Paul F. Quigley and Stanley M. Roberts pg 1809; DOI: 10.1039/b002704i |
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Carbon–carbon bond formation via thermal intermolecular hydrogen atom transfer: two serendipitous heterocyclic examples Richard J. Hamlyn Richard H. Jones and Christopher A. Ramsden pg 1811; DOI: 10.1039/a909891g |
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Oxygen to carbon rearrangements of anomerically linked alkenols from tetrahydropyran derivatives: an investigation of the reaction mechanism via a double isotopic labelling crossover study Marianne F. Buffet Darren J. Dixon Gavin L. Edwards Steven V. Ley and Edward W. Tate pg 1815; DOI: 10.1039/a909300a |
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The synthesis of mono- and bicyclic ethers via acid catalysed ring-opening cyclisation of tetrahydropyranyl ether derivatives Darren J. Dixon Steven V. Ley and Edward W. Tate pg 1829; DOI: 10.1039/a909302h |
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A flexible and efficient synthesis of the pyrrolidine -glycosidase inhibitor 1,4-dideoxy-1,4-imino-D-arabinitol (DAB-1) Alison N. Hulme Charles H. Montgomery and David K. Henderson pg 1837; DOI: 10.1039/b002707n |
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Synthesis of 7-substituted 3-aryl-1,6-naphthyridin-2-amines and 7-substituted 3-aryl-1,6-naphthyridin-2(1H)-ones via diazotization of 3-aryl-1,6-naphthyridine-2,7-diamines Andrew M. Thompson H. D. Hollis Showalter and William A. Denny pg 1843; DOI: 10.1039/b002599m |
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Synthesis of benzolactams by 11-endo selective aryl radical cyclisation of 2-iodobenzamides Maria A. F. Prado Ricardo J. Alves José D. Souza Filho Rosemeire B. Alves Maria T. C. Pedrosa Renata F. Prado and André A. G. Faraco pg 1853; DOI: 10.1039/b002416n |
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Thio-oligosaccharides of sialic acid – synthesis of an ( W. Bruce Turnbull and Robert A. Field pg 1859; DOI: 10.1039/b002319l |
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Multicomponent synthesis of tripeptides containing pipecolic acid derivatives: selective induction of cis- and trans-imide bonds into peptide backbones Wolfgang Maison Arne Lützen Marc Kosten Imre Schlemminger Ole Westerhoff Wolfgang Saak and Jürgen Martens pg 1867; DOI: 10.1039/b002258f |
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Concise synthesis of azacycloundecenes using ring-closing metathesis (RCM) Mitsuhiro Arisawa Chiaki Kato Hiroaki Kaneko Atsushi Nishida and Masako Nakagawa pg 1873; DOI: 10.1039/b002117m |
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An effective self-templating ring closure method for mixed donor thiophene-based macrocycles Joan Halfpenny and Zachary S. Sloman pg 1877; DOI: 10.1039/b002029j |
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Synthesis and characterisation of water-soluble poly(aryl ether) dendrimers for encapsulation of biomimetic active site analogues Michael J. Hannon Paul C. Mayers and Paul C. Taylor pg 1881; DOI: 10.1039/b002026p |
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Rhodium(II)-carbenoid C–H insertion reactions in the synthesis of Pompiliu S. Aburel and Kjell Undheim pg 1891; DOI: 10.1039/b001988g |
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Optically active 1,5-benzothiazepin-4-ones by ring transformation of 5-ylidene-1,3-dioxan-4-ones with 2-aminothiophenol Akbar Ali Viqar Uddin Ahmad Joachim Leistner and Jürgen Liebscher pg 1897; DOI: 10.1039/b001928n |
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Stereochemically controlled synthesis of 1,8-dioxaspiro[4.5]decanes and 1-oxa-8-thiaspiro[4.5]decanes by phenylsulfanyl migration Jason Eames David J. Fox Maria A. de las Heras and Stuart Warren pg 1903; DOI: 10.1039/b001893g |
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Palladium(II)-catalyzed oxidation of terminal alkenes to methyl ketones using molecular oxygen Takahiro Nishimura Nobuyuki Kakiuchi Tomoaki Onoue Kouichi Ohe and Sakae Uemura pg 1915; DOI: 10.1039/b001854f |
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Vinylogous urethanes in alkaloid synthesis. Applications to the synthesis of racemic indolizidine 209B and its (5R*,8S*,8aS*)-() diastereomer, and to (–)-indolizidine 209B Joseph P. Michael and David Gravestock pg 1919; DOI: 10.1039/b001853h |
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Reactions of polyfluorinated cyclohexadienones with diazoalkanes. Part 1. Formation of cyclopropanes from polyfluorinated cyclohexa-2,4-dienones with diazomethane and phenyldiazomethane Vladimir N. Kovtonyuk Ljubov S. Kobrina Yurij V. Gatilov Irina Yu. Bagryanskaya Roland Fröhlich and Günter Haufe pg 1929; DOI: 10.1039/b001618g |
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Synthesis of adenophostin A and congeners modified at glucose Rachel D. Marwood Andrew M. Riley David J. Jenkins and Barry V. L. Potter pg 1935; DOI: 10.1039/b001386m |
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Cyclohexyl ether as a new hydroxy-protecting group for serine and threonine in peptide synthesis Yasuhiro Nishiyama Suguru Shikama Ken-ichi Morita and Keisuke Kurita pg 1949; DOI: 10.1039/b001261k |
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Nitrogen substituted cyclic enediynes: synthesis, thermal reactivity and complexation with metal ions Amit Basak Jagadish Chandra Shain Uttam Kumar Khamrai Kakali Rani Rudra and Ajoy Basak pg 1955; DOI: 10.1039/b000963f |
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An alternative general preparation of 2-alkyl-1-benzostannepines and their conversion into 1-benzostibepines and 1-benzoborepines via a tin–metal exchange Haruki Sashida and Atsuhiro Kuroda pg 1965; DOI: 10.1039/b000900h |
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A 2,3,5,6-tetramethylenebicyclo[2.2.0]hexane derivative: a novel bisdiene molecule that produces a Dewar benzene skeleton upon two successive Diels–Alder reactions with dienophiles Masakazu Ohkita Kieko Sano Sotoyuki Dohba Yuko Fujita Takanori Suzuki and Takashi Tsuji pg 1971; DOI: 10.1039/b000569j |
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On the diastereoselectivity of alkylations of bicyclic lactams Jonathan H. Bailey Andrew T. J. Byfield Philip J. Davis Alison C. Foster Michael Leech Mark G. Moloney Matthias Müller and C. Keith Prout pg 1977; DOI: 10.1039/b000432o |
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Preparation of chiral enantiopure 2-(hydroxyalkyl)pyridine derivatives. Use of the chiral pool Fredrik Rahm Robert Stranne Ulf Bremberg Kerstin Nordström Magnus Cernerud Emmanuel Macedo and Christina Moberg pg 1983; DOI: 10.1039/b000269k |
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The mechanism of [2+1] and [2+2] cycloaddition reactions of 1-phenylseleno-2-(trimethylsilyl)ethene: an isotopic labelling study Shoko Yamazaki Yuichiro Yanase and Kagetoshi Yamamoto pg 1991; DOI: 10.1039/a909919k |
Issue 13
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Perkin 1 Abstracts: Solid Phase Organic Synthesis John Christopher Catherine McCusker Fiona McKerlie Tanya Wildman Jason Tierney and Bernard Wathey pg 13-vii; DOI: 10.1039/b004202l |
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Metals as surrogates for hydrogen in organic chemistry: anything hydrogen can do, a metal can do better Alwyn G. Davies pg 1997; DOI: 10.1039/a909835f |
The influence of boric acid on the acetylation of aldoses:  one-pot syntheses of penta-O-acetyl--D-glucofuranose and its crystalline propanoyl analogueRichard H. Furneaux Phillip M. Rendle and Ian M. Sims pg 2011; DOI: 10.1039/b002841j |
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Preparation of N-(alk-1-enyl) nucleobase compounds by Horner and Horner–Wadsworth–Emmons reactions Thomas Boesen Christian Madsen Ulla Henriksen and Otto Dahl pg 2015; DOI: 10.1039/b002744h |
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Synthesis and in vitro enzyme activity of peptide derivatives of bacterial cell wall biosynthesis inhibitors Russell J. Cox Helen Jenkins James A. Schouten Rosie A. Stentiford and Katrina J. Wareing pg 2023; DOI: 10.1039/b002701o |
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Ritter reactions. Part 14. Rearrangement of 3,3,7,7-tetramethyl-6-methylidenebicyclo[3.3.1]nonan-2-one Djamal Djaidi Ivy S. H. Leung Roger Bishop Donald C. Craig and Marcia L. Scudder pg 2037; DOI: 10.1039/b002544p |
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Triterpenoid total synthesis. Part 5. Synthetic disproof of the triterpene structure proposed for naurol A, a cytotoxic metabolite of a Pacific sponge Dai Nozawa Hirosato Takikawa and Kenji Mori pg 2043; DOI: 10.1039/b002500n |
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Observations on the ring opening reactions of 2-methyleneaziridines with acid chlorides and alkyl chloroformates David S. Ennis Julie Ince Sabitur Rahman and Michael Shipman pg 2047; DOI: 10.1039/b002223n |
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Polystyrene and polymethacrylate resin-supported Jacobsens alkene epoxidation catalyst Laetitia Canali Elaine Cowan Hervé Deleuze Colin L. Gibson and David C. Sherrington pg 2055; DOI: 10.1039/b002118k |
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Stereoselective synthesis of C-4-aminouridines (uracil C-4-amino-D-ribonucleosides) Masataka Yokoyama Taku Ikenogami and Hideo Togo pg 2067; DOI: 10.1039/b002063j |
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A practical total synthesis of plaunotol via highly Z-selective Wittig olefination of -acetal ketones Keiko Tago Masami Arai and Hiroshi Kogen pg 2073; DOI: 10.1039/b001977l |
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Crystal structure of vinblastine Robert Bau and Kevin Kai Jin pg 2079; DOI: 10.1039/b001855o |
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Synthesis of syn-3a(12c),9a(9b)-dihomoperylene-3,10-dione, (E)-syn-2,2-bi(7H-1,6-methano[10]annulenylidene)-7,7-dione and of its rearrangement product, trans-12a,12b-dihydro-3a(12c),9a(9b)-dihomoperylene-3,10-dione Aderson de Farias Dias Thomas Helwig Johann Lex Joseph Miller and Hans Schmickler pg 2083; DOI: 10.1039/b001786h |
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Chemo-enzymatic synthesis of glycopolymers and sequential glycopeptides bearing lactosamine and sialyl Lewisx unit pendant chains Florence Sallas and Shin-Ichiro Nishimura pg 2091; DOI: 10.1039/b001612h |
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Stereoselective synthesis of trans-2,6-diaryl-4-piperidones by using benzaldiminetricarbonylchromium derivatives Kaori Ishimaru and Takakazu Kojima pg 2105; DOI: 10.1039/b001540g |
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The reactions of diazo compounds with lactones. Part 1. Cyclopropanespiro--lactones from diketene: synthesis and reactions Paul V. Murphy Timothy J. O Sullivan and Niall W. A. Geraghty pg 2109; DOI: 10.1039/b001393p |
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The reactions of diazo compounds with lactones. Part 2. The reaction of cyclic 2-diazo-1,3-dicarbonyl compounds with diketene: benzofuran formation Paul V. Murphy Timothy J. O Sullivan Bryan D. Kennedy and Niall W. A. Geraghty pg 2121; DOI: 10.1039/b001394n |
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Synthesis and application of sialic acid-containing building blocks for glycopeptide libraries. Establishing glycosylation conditions Koen M. Halkes Phaedria M. St. Hilaire Anita M. Jansson Charlotte H. Gotfredsen and Morten Meldal pg 2127; DOI: 10.1039/a908321i |
Issue 14
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Perkin 1 Abstracts: Natural Product Synthesis Robert Narquizian Jacqueline Milne and Duncan McArthur pg 14-ix; DOI: 10.1039/b004204h |
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Recent developments in oligosaccharide synthesis Benjamin G. Davis pg 2137; DOI: 10.1039/a809774g |
 3-1,3,4-Oxadiazolines. Versatile sources of reactive intermediatesJohn Warkentin pg 2161; DOI: 10.1039/b000930j |
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Highly site-selective alkylation reaction of bent aza-heterocycles by alkyllithium and alkyl halides Dipanjan Pan Bidhan C. Roy Gandhi K. Kar and Jayanta K. Ray pg 2171; DOI: 10.1039/b003492o |
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-Allyl cation cyclisations initiated by silver(I)-promoted electrocyclic ring opening of ring-fused gem-dibromocyclopropanes possessing tethered nucleophiles: the influence of chiral auxiliaries on the diastereoselectivity of cyclisations involving meso-substrates Martin Banwell Alison Edwards Joanne Harvey David Hockless and Anthony Willis pg 2175; DOI: 10.1039/b002525i |
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Indium-mediated facile synthesis of 3-unsubstituted -lactams Bimal K. Banik Anjan Ghatak and Frederick F. Becker pg 2179; DOI: 10.1039/b002833i |
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Synthesis, structure and reactivity of a trifluoromethyl sulfide anionic salt stabilized with tetrakis(dimethylamino)ethylene dication (TDAE2+) Alexander Kolomeitsev Maurice Médebielle Peer Kirsch Enno Lork and Gerd-Volker Röschenthaler pg 2183; DOI: 10.1039/b002252g |
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Stereoselective synthesis of -L-Fucp-(1,2)- and -(1,3)--D-Galp(1)-4-methylumbelliferone using glycosyl donor substituted by propane-1,3-diyl phosphate as leaving group Hariprasad Vankayalapati and Gurdial Singh pg 2187; DOI: 10.1039/b002754p |
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Regio- and stereo-selective bromo(alkoxylation)s of (E)--(2,3,4,6-tetra-O-acetyl--D-glucopyranosyloxymethylene) carbonyl compounds. A route to near-stereopure -bromo -dioxymethyl carbonyl compounds M. Sum Idris David S. Larsen Robin G. Pritchard Anthony Schofield Richard J. Stoodley and Peter D. Tiffin pg 2195; DOI: 10.1039/b002749i |
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Studies in the cycloproparene series: chemistry of 1H-cyclopropa[b]naphthalene-3,6-dione and its transformation into 1H-cyclopropa[b]anthracene-3,8-dione1 Brian Halton Carissa S. Jones Andrew J. Kay Davor Margetic and Sanja Sretenovic pg 2205; DOI: 10.1039/b002683m |
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Synthesis of (3S*,4R*,6E,10Z)-3,4,7,11-tetramethyltrideca-6,10-dienal (faranal) using stereospecific 1,4-cis-hydrogenation of conjugated double bonds Andrei A. Vasil ev Lars Engman and Edward P. Serebryakov pg 2211; DOI: 10.1039/b002343o |
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Difference in guest-inclusion abilities of anti- and syn-rotamers Keiki Kishikawa Chiaki Iwashima Shigeo Kohmoto Kentaro Yamaguchi and Makoto Yamamoto pg 2217; DOI: 10.1039/b002220i |
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Highly selective acylation of alcohols and amines by an indium triiodide-catalysed transesterification process Brindaban C. Ranu Pinak Dutta and Arunkanti Sarkar pg 2223; DOI: 10.1039/b002181o |
Preparation and cleavage reactions of 3-thiouridylyl-(3 5)-uridineXiaohai Liu and Colin B. Reese pg 2227; DOI: 10.1039/b002155p |
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Practical syntheses of [13C]- and [14C]-labelled glucosphingolipids Gordon R. Duffin George J. Ellames Sascha Hartmann John M. Herbert and David I. Smith pg 2237; DOI: 10.1039/b002104k |
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Use of the Wadsworth–Emmons reaction for preparing hindered vinyl ethers and related 1,2-dioxetanes Carl A. Roeschlaub and Peter G. Sammes pg 2243; DOI: 10.1039/b002101f |
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Synthesis and conjugation of oligosaccharide fragments related to the immunologically reactive part of the circulating anodic antigen of the parasite Schistosoma mansoni Henricus J. Vermeer Koen M. Halkes J. Albert van Kuik Johannis P. Kamerling and Johannes F. G. Vliegenthart pg 2249; DOI: 10.1039/b002083o |
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Study of a tandem aldol–Tischtschenko reaction between chiral enolsilanes and aldehydes catalyzed by titanium(IV) isopropoxide Christophe Delas Olivier Blacque and Claude Moïse pg 2265; DOI: 10.1039/b002008g |
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Syntheses of some polyunsaturated trifluoromethyl ketones as potential phospholipase A2 inhibitors Anne Kristin Holmeide and Lars Skattebøl pg 2271; DOI: 10.1039/b001944p |
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Photosensitized oxidation, by single-electron transfer, of catharanthine and vindoline: a highly regio- and diastereoselective photocyanation reaction Guillaume Cocquet Patrice Rool and Clotilde Ferroud pg 2277; DOI: 10.1039/b001114m |
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Dismutation of aldehydes catalyzed by alcohol dehydrogenases Kelly Velonia and Ioulia Smonou pg 2283; DOI: 10.1039/b001039l |
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The preparation and some properties of substituted phenylene-ethynylene and phenylenebuta-1,3-diynylene polymers Andrew Pelter and D. Elfyn Jones pg 2289; DOI: 10.1039/a908642k |
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Heterocalixarenes Part 4. Synthesis of oxocalix[1]heterocycle[2]arenes: a unique H-bonding network in calix[1]benzimidazol-2-one[2]arene12 H2O Subodh Kumar Geeta Hundal Dharam Paul Maninder Singh Hundal and Harjit Singh pg 2295; DOI: 10.1039/b000832j |
Issue 15
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Leslie Crombie Donald A. Whiting pg 2303; DOI: 10.1039/b004067n |
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Facile and highly selective 5-desilylation of multisilylated nucleosides Xue-Feng Zhu Howard J. Williams and A. Ian Scott pg 2305; DOI: 10.1039/b003562i |
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The structure of laricinolic acid and its biomimetic transformation into officinalic acid Bernhard Erb Hans-Jürg Borschberg and Duilio Arigoni pg 2307; DOI: 10.1039/b001984o |
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The synthesis of novel heterocyclic substituted -amino acids; further exploitation of -amino acid alkynyl ketones as reactive substrates Robert M. Adlington Jack E. Baldwin David Catterick Gareth J. Pritchard and Lam T. Tang pg 2311; DOI: 10.1039/b001825m |
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Stereochemistry of the decarboxylation of glyoxylic acid by yeast pyruvate decarboxylase Hiran Vegad Mario Lobell Stephen Bornemann and David H. G. Crout pg 2317; DOI: 10.1039/b002504f |
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A liquid chromatography–thermospray ionisation–mass spectrometry guided isolation of a new sesquiterpene aryl ester from Armillaria novae-zelandiae Peadar Cremin Patrick J. Guiry Jean-Luc Wolfender Kurt Hostettmann and Dervilla M. X. Donnelly pg 2325; DOI: 10.1039/b001980l |
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Synthesis of imidazo[1,2-a]pyridines from unactivated 2-alkyl-4,5-dihydroimidazoles through conjugate N-addition Raymond C. F. Jones Paschalis Dimopoulos Simon C. Coles Mark E. Light and Michael B. Hursthouse pg 2331; DOI: 10.1039/b001830i |
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1-Aminobenzotriazole functionalisation using directed metallation: new routes to chromanes and chromenes using intramolecular benzyne trapping by alcohols David W. Knight and Paul B. Little pg 2343; DOI: 10.1039/b001834l |
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Synthetic studies on the pederin family of antitumour agents. Syntheses of mycalamide B, theopederin D and pederin Philip Kocienski Robert Narquizian Piotr Raubo Christopher Smith Louis J. Farrugia Kenneth Muir and F. Thomas Boyle pg 2357; DOI: 10.1039/a909898d |
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Diastereoselective oxygen to carbon rearrangements of anomerically linked enol ethers and the total synthesis of (+)-(S,S)-(cis-6-methyltetrahydropyran-2-yl)acetic acid, a component of civet Darren J. Dixon Steven V. Ley and Edward W. Tate pg 2385; DOI: 10.1039/b001243m |
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A radical based addition–elimination route for the preparation of indoles John A. Murphy Karen A. Scott Rhona S. Sinclair Concepcion Gonzalez Martin Alan R. Kennedy and Norman Lewis pg 2395; DOI: 10.1039/b002565h |
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Absolute configurational assignment of 3-hydroxycarotenoids Thomas Andersson Babak Borhan Nina Berova Koji Nakanishi Jarle Andre Haugan and Synnøve Liaaen-Jensen pg 2409; DOI: 10.1039/b002088p |
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Towards a total synthesis of ulapualide A. Concise synthetic routes to the tris-oxazole ring system and tris-oxazole macrolide core in ulapualides, kabiramides, halichondramides, mycalolides and halishigamides Shital K. Chattopadhyay James Kempson Alan McNeil Gerald Pattenden Michael Reader David E. Rippon and David Waite pg 2415; DOI: 10.1039/b000750l |
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A total synthesis of the unique tris-oxazole macrolide ulapualide A produced by the marine nudibranch Hexabranchus sanguineus Shital K. Chattopadhyay and Gerald Pattenden pg 2429; DOI: 10.1039/b000751j |
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Stereocontrolled ring-opening of some enantiomerically enriched epoxy ketones and epoxy alcohols using trimethylaluminium: synthesis of (S)-2-arylpropanoic acids Lydia Carde D. Huw Davies and Stanley M. Roberts pg 2455; DOI: 10.1039/b000996m |
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Asymmetric synthesis of amino sugars. Part 2. A novel versatile approach to the chiral non-racemic synthesis of 2-amino-2-deoxy sugars. Preparation of L-glucosamine, L-mannosamine and L-talosamine derivatives Ludmila Ermolenko N. André Sasaki and Pierre Potier pg 2465; DOI: 10.1039/b001721n |
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Structure elucidation and synthesis of (4S,5S,6Z,8E)-5-hydroxydeca-6,8-dien-4-olide [(S,S)-sapinofuranone B]—a novel -lactone metabolite of Acremonium strictum Sarah Clough Mairi E. Raggatt Thomas J. Simpson Christine L. Willis Andrew Whiting and Stephen K. Wrigley pg 2475; DOI: 10.1039/b001823f |
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Stereoselective total syntheses of atrochrysone, torosachrysone and related 3,4-dihydroanthracen-1(2H)-ones Michael Müller Kai Lamottke Erich Löw Eva Magor-Veenstra and Wolfgang Steglich pg 2483; DOI: 10.1039/b003053h |
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Stereoselectivity, regioselectivity and mechanism in the intramolecular citran bicyclisation of chromenes Cesar Calderon-Higginson Leslie Crombie Sally D. Redshaw and Donald A. Whiting pg 2491; DOI: 10.1039/b001310m |
Issue 16
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Perkin 1 Abstracts: Solid Phase Organic Synthesis Catherine McCusker Fiona McKerlie Tanya Wildman Jason Tierney and Bernard Wathey pg 16-xi; DOI: 10.1039/b004800n |
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Perkin 1 Abstracts: Natural Product Synthesis Duncan McArthur and Jacqueline Milne pg 16-xxii; DOI: 10.1039/b004801l |
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Perkin 1 Abstracts: Biocatalysis in Organic Synthesis Gideon Grogan Alexis Carstairs Ian Jackson Denise McIntyre Alan Watt Sabine Flitsch and Nicholas Turner pg 16-xv; DOI: 10.1039/b004955g |
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Protecting groups Krzysztof Jarowicki and Philip Kocienski pg 2495; DOI: 10.1039/b003410j |
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Alcohols, ethers and phenols Trevor George Ross Mabon Gemma Sweeney J. B. Sweeney and Ali Tavassoli pg 2529; DOI: 10.1039/a808133f |
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Alkylation of peroxyacids as a new method of peroxyester synthesis Stefan Baj and Anna Chrobok pg 2575; DOI: 10.1039/b005192f |
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Domino Michael–seleno Pummerer type reaction (additive seleno Pummerer reaction) Hisahiro Hagiwara Koji Kafuku Hitoshi Sakai Miki Kirita Takashi Hoshi Toshio Suzuki and Masayoshi Ando pg 2577; DOI: 10.1039/b004912n |
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Chemoenzymatic synthesis of a biotin-labeled glycophosphononapeptide of the c-Myc oncoprotein Thomas Kappes-Roth and Herbert Waldmann pg 2579; DOI: 10.1039/b004822o |
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An enantiospecific approach to pinguisanes from (R)-carvone. Total synthesis of (+)-pinguisenol Adusumilli Srikrishna and Dange Vijaykumar pg 2583; DOI: 10.1039/b004770h |
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Facile syntheses of building blocks for the construction of phosphotyrosine mimetics G. Stuart Cockerill Howard J. Easterfield Jonathan M. Percy and Stéphane Pintat pg 2591; DOI: 10.1039/b004187o |
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Cyclisation chemistry of 4H-1,2,6-thiadiazines Panayiotis A. Koutentis and Charles W. Rees pg 2601; DOI: 10.1039/b004113k |
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Coupling reactions of indole-3-acetic acid derivatives. Synthesis of arcyriaflavin A Jan Bergman Eva Koch and Benjamin Pelcman pg 2609; DOI: 10.1039/b004029k |
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Acid-induced dimerization of 3-(1H-indol-3-yl)maleimides. Formation of cyclopentindole derivatives Jan Bergman Tomasz Janosik Eva Koch and Benjamin Pelcman pg 2615; DOI: 10.1039/b004030o |
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Preparation and structures of novel [2.2.2]metacyclophane tweezers Tsuyoshi Sawada Masaki Yamada Thies Thiemann and Shuntaro Mataka pg 2623; DOI: 10.1039/b003584j |
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Asymmetric total synthesis of (+)-equilenin utilizing two types of cascade ring expansion reactions of small ring systems Masahiro Yoshida Mohamed Abdel-Hamid Ismail Hideo Nemoto and Masataka Ihara pg 2629; DOI: 10.1039/b003578p |
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Synthesis of N-aryl-substituted iminophosphoranes and NMR spectroscopic investigation of their acid–base properties in acetonitrile Toomas Rodima Vahur Mäemets and Ilmar Koppel pg 2637; DOI: 10.1039/b003575k |
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Total synthesis of a monocyclofarnesane dinorsesquiterpenoid isolated from mushroom ingested by beetle: Selectivity in solid-state Baeyer–Villiger reaction Hisahiro Hagiwara Hidenori Nagatomo Fumiko Yoshii Takashi Hoshi Toshio Suzuki and Masayoshi Ando pg 2645; DOI: 10.1039/b003571h |
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Regio- and diastereo-selectivity in 1,3-dipolar cycloadditions of nitrile oxides to 4-substituted cyclopent-2-enones Giorgio Adembri Gianluca Giorgi Raffaella L. Lampariello Maria L. Paoli and Alessandro Sega pg 2649; DOI: 10.1039/b003549l |
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Synthesis of (+)- and (–)-ferruginol via asymmetric cyclization of a polyene Masahiro Tada Sei Nishiiri Yang Zhixiang Yumiko Imai Shiho Tajima Naoko Okazaki Yoshikazu Kitano and Kazuhiro Chiba pg 2657; DOI: 10.1039/b003497p |
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Biosynthesis of kendomycin: origin of the oxygen atoms and further investigations Helge B. Bode and Axel Zeeck pg 2665; DOI: 10.1039/b003362f |
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Synthesis and coplanarity-dependent HOMO–LUMO separation of -conjugated dimers Takashi Murashima Daiki Shiga Keiji Nishi Hidemitsu Uno and Noboru Ono pg 2671; DOI: 10.1039/b003211p |
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Synthesis of trimethylgermyl trimethylsilyl ketone and bis(trimethylgermyl) ketone Rune Johannesen and Tore Benneche pg 2677; DOI: 10.1039/b003016n |
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Synthesis of the bisbenzannelated spiroketal core of the -rubromycins. The use of a novel Nef-type reaction mediated by Pearlmans catalyst Tanya Capecchi Charles B. de Koning and Joseph P. Michael pg 2681; DOI: 10.1039/b002984j |
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Friedel–Crafts sulfonylation of aromatics catalysed by solid acids: An eco-friendly route for sulfone synthesis Boyapati M. Choudary N. Sreenivasa Chowdari and M. Lakshmi Kantam pg 2689; DOI: 10.1039/b002931i |
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Synthesis of 1,3,5-tris[4-(diarylamino)phenyl]benzene and 1,3,5-tris(diarylamino)benzene derivatives M. John Plater Murray McKay and Toby Jackson pg 2695; DOI: 10.1039/b002928i |
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Biosynthesis of kelsoene and prespatane in cultured cells of the liverwort Ptychanthus striatus Kensuke Nabeta Masateru Yamamoto Kanako Fukushima and Kenji Katoh pg 2703; DOI: 10.1039/b002843f |
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Chemical synthesis of -D-GlcpA(2SO4)-(13)-D-GalpNAc(6SO4), the disaccharide repeating unit of shark cartilage chondroitin sulfate D, and of its methyl -D-glycoside derivative Nathalie Karst and Jean-Claude Jacquinet pg 2709; DOI: 10.1039/b002835p |
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Electrochemical oxidative coupling of 1,4-bis(1,4-dithiafulven-6-yl)benzene cyclophanes Dominique Lorcy David Guérin Kamal Boubekeur Roger Carlier Philippe Hascoat André Tallec and Albert Robert pg 2719; DOI: 10.1039/b002596h |
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Nickel(0)-catalysed asymmetric cross-coupling reactions of allylic compounds with Grignard reagents using optically active oxazolinylferrocenylphosphines as ligands Kang-Go Chung Yoshihiro Miyake and Sakae Uemura pg 2725; DOI: 10.1039/b002547j |
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Neighboring effect of pyrazole rings: regio- and stereoselective Wagner–Meerwein rearrangement in electrophilic addition reactions of norbornadiene-fused pyrazoles Tomoshige Kobayashi and Yosuke Uchiyama pg 2731; DOI: 10.1039/b002454f |
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Studies on piezochromic photochromic (E)-5-dicyanomethylene-3-[1-(2,5-dimethyl-3-furyl)ethylidene]-4-diphenylmethylenetetrahydrofuran-2-one and related photochromic compounds Abdullah M. A. Asiri Alison Cleeves and Harry G. Heller pg 2741; DOI: 10.1039/b002414g |
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Highly efficient and selective electrophilic and free radical catalytic bromination reactions of simple aromatic compounds in the presence of reusable zeolites Keith Smith Gamal A. El-Hiti Mark E. W. Hammond Dawoud Bahzad Zhaoqiang Li and Christophe Siquet pg 2745; DOI: 10.1039/b002157l |
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A novel method for the nitration of deactivated aromatic compounds Keith Smith Tracy Gibbins Ross W. Millar and Robert P. Claridge pg 2753; DOI: 10.1039/b002158j |
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Enantioselective synthesis of -bromo acid derivatives and bromohydrins from tartrate derived bromoacetals Scott A. Boyes and Alan T. Hewson pg 2759; DOI: 10.1039/b002106g |
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Synthesis of novel 1-methylindole trimer and tetramer under Friedel–Crafts reaction conditions and determination of their structures by X-ray crystallography Shashi B. Mahato Subhadra Garai Manuela Weber and Peter Luger pg 2767; DOI: 10.1039/b002074p |
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NMR studies of tautomerism in the fungal melanin biosynthesis intermediate 1,3,8-trihydroxynaphthalene Thomas J. Simpson and M. K. Bandumathie Weerasooriya pg 2771; DOI: 10.1039/b002030n |
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Synthesis and properties of stable heteroazulene analogues of a triphenylmethyl cation Shin-ichi Naya and Makoto Nitta pg 2777; DOI: 10.1039/b002025g |
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Pyrrolidinones derived from (S)-pyroglutamic acid. Part 1. Conformationally constrained glutamate Jonathan H. Bailey David T. Cherry James Dyer Mark G. Moloney Mark J. Bamford Steve Keeling and R. Brian Lamont pg 2783; DOI: 10.1039/b001999m |
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Pyrrolidinones derived from (S)-pyroglutamic acid. Part 2. Conformationally constrained kainoid analogues James Dyer Amanda King Steve Keeling and Mark G. Moloney pg 2793; DOI: 10.1039/b002001j |
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The synthesis and structural characterization of the first bis(benzocrown ethers) with polyyne linkages Liang-Hui Lee Vincent Lynch and Richard J. Lagow pg 2805; DOI: 10.1039/b001856m |
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Problems in the synthesis of cyclic peptides through use of the Dmab protecting group Tony Johnson Mark Liley Timothy J. Cheeseright and Farida Begum pg 2811; DOI: 10.1039/b001694m |
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Asymmetric reduction of ethynyl ketones and ethynylketoesters by secondary alcohol dehydrogenase from Thermoanaerobacter ethanolicus Christian Heiss and Robert S. Phillips pg 2821; DOI: 10.1039/b001329n |
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Indium triflate: a new catalyst for (4+2)-cycloaddition of chromone Schiffs bases Sunil Gadhwal and Jagir S. Sandhu pg 2827; DOI: 10.1039/b000923g |
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Synthesis of model compounds for potential contrast agents containing phosphonate and peptide moieties Hutti Shalem Shimon Shatzmiller and Ben-Ami Feit pg 2831; DOI: 10.1039/a909086j |
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Synthesis and biological resolution of condensed bicyclic isoparaconic acid derivatives Sara Drioli Fulvia Felluga Cristina Forzato Giuliana Pitacco and Ennio Valentin pg 2839; DOI: 10.1039/b001615m |
Issue 17
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Solid Phase Organic Synthesis Catherine McCusker Fiona McKerlie Tanya Wildman Jason Tierney and Bernard Wathey pg 17-ix; DOI: 10.1039/b005971o |
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Rapid analogue syntheses of heteroaromatic compounds Ian Collins pg 2845; DOI: 10.1039/a904715h |
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Saturated nitrogen heterocycles Andrew Mitchenson and Alan Nadin pg 2862; DOI: 10.1039/a908537h |
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C-18 Hydroxylation of gibberellins Lewis N. Mander and Regan J. Thomson pg 2893; DOI: 10.1039/b006044p |
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A new reaction of 1-(2,4,6-trialkylphenyl)phospholes with heteroaromatic character; aromatic electrophilic substitution under the conditions of Friedel–Crafts acylation György Keglevich Tungalag Chuluunbaatar Beáta Dajka András Dobó Áron Szöllsy and László Töke pg 2895; DOI: 10.1039/b004695g |
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A novel annelation to quinolines and isoquinolines under Friedel–Crafts conditions: a one-step synthesis of functionalized pyridoquinolines and pyridoisoquinolines Shashi B. Mahato Subhadra Garai Manuela Weber and Peter Luger pg 2898; DOI: 10.1039/b004444j |
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An activated phosphate for an efficient amide and peptide coupling reagent Tomohisa Yasuhara Yasuo Nagaoka and Kiyoshi Tomioka pg 2901; DOI: 10.1039/b004264l |
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Synthesis and anti-HIV-1 activity of novel bicyclic nucleoside analogues restricted to an S-type conformation Lisbet Kvrnø Claus Nielsen and Richard H. Wightman pg 2903; DOI: 10.1039/b004774k |
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The synthesis and properties of Gla- and Phe-containing analogues of cyclic RGD pentapeptides John S. Davies Christine Enjalbal Corrine Nguyen Loai Al-Jamri and Christian Naumer pg 2907; DOI: 10.1039/b004677i |
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Single and double ring closing metathesis in the formation of dihydropyrans and bisoxacyclic systems with a quaternary centre Bernd Schmidt and Holger Wildemann pg 2916; DOI: 10.1039/b004302h |
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Synthesis of N,N-bis(silyloxy)enamines with a functionalized double bond Alexander D. Dilman Alexander A. Tishkov Il ya M. Lyapkalo Sema L. Ioffe Vadim V. Kachala Yury A. Strelenko and Vladimir A. Tartakovsky pg 2926; DOI: 10.1039/b004268o |
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Synthesis of some thiochromeno[4,3-c]- and [3,4-c]-pyrazoles Christopher D. Gabbutt John D. Hepworth B. Mark Heron Simon J. Coles and Michael B. Hursthouse pg 2930; DOI: 10.1039/b004149l |
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A novel oxidative alkylation–nitration of 1,3-dicarbonyl compounds to dicyclopentadiene and norbornene Bor-Cherng Hong Hsu-I Sun Yeong-Jou Shr and Kuan-Jiuh Lin pg 2939; DOI: 10.1039/b004095i |
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Synthesis and conformational analysis of a dimerising eight-membered lactam dipeptide Sam Derrer John E. Davies and Andrew B. Holmes pg 2943; DOI: 10.1039/b003789n |
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Synthesis and conformational analysis of a type VIb -turn mimetic based on an eight-membered lactam Sam Derrer John E. Davies and Andrew B. Holmes pg 2957; DOI: 10.1039/b003791p |
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[4+2] Cycloaddition of thiophene S-monoxides to activated methylenecyclopropanes Thies Thiemann Daisuke Ohira Yuanqiang Li Tsuyoshi Sawada Shuntaro Mataka Karsten Rauch Mathias Noltemeyer and Armin de Meijere pg 2968; DOI: 10.1039/b003850o |
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Preparation of 5-unsubstituted 4-formylpyrrole-2-carboxylates and conversion to cycloalkano-oligopyrroles Yumiko Fumoto Hidemitsu Uno Satoshi Ito Yuka Tsugumi Maki Sasaki Yukiko Kitawaki and Noboru Ono pg 2977; DOI: 10.1039/b003360j |
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Chirally templated boronic acid Mannich reaction in the synthesis of optically active -amino acids Gordon S. Currie Michael G. B. Drew Laurence M. Harwood David J. Hughes Richard W. A. Luke and Richard J. Vickers pg 2982; DOI: 10.1039/b003067h |
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Bu3SnH mediated oxidative radical cyclisations: synthesis of 6H-benzo[c]chromen-6-ones W. Russell Bowman Emma Mann and Jonathan Parr pg 2991; DOI: 10.1039/b002539i |
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Synthesis and anti-influenza virus activity of novel glycopolymers having triantennary oligosaccharide branches Tetsuya Furuike Seiichi Aiba Takashi Suzuki Tadanobu Takahashi Yasuo Suzuki Kuriko Yamada and Shin-Ichiro Nishimura pg 3000; DOI: 10.1039/b002412k |
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Selectivity in Lewis acid-mediated fragmentations of peroxides and ozonides: application to the synthesis of alkenes, homoallyl ethers, and 1,2-dioxolanes Patrick H. Dussault Hyung-Jae Lee and Xuejun Liu pg 3006; DOI: 10.1039/b001391i |
Issue 18
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Perkin 1 Abstracts: Biocatalysis in Organic Synthesis Gideon Grogan Alexis Carstairs Ian Jackson Denise McIntyre Alan Watt Sabine Flitsch and Nicholas Turner pg 18-ix; DOI: 10.1039/b005914p |
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Perkin 1 Abstracts: Natural Product Synthesis Jacqueline E. Milne Marcel de Puit and Duncan McArthur pg 18-xv; DOI: 10.1039/b006702o |
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Advances in indium-catalysed organic synthesis Kamlesh K. Chauhan and Christopher G. Frost pg 3015; DOI: 10.1039/a906657h |
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A new reaction of electron-rich thiophenemethanols R. Alan Aitken and Alasdair N. Garnett pg 3020; DOI: 10.1039/b006513g |
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Photoreactions of -aziridinylacrylonitrile. 1,3-Dipolar cycloadditions of photoinduced azomethine ylide Keitaro Ishii Yukio Shimada Shigeo Sugiyama and Masahiro Noji pg 3022; DOI: 10.1039/b004850j |
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Strategies for protodesilylation of C-2 trialkylsilyl terminal alkenes James C. Anderson and Alice Flaherty pg 3025; DOI: 10.1039/b006049f |
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The use of -allyltricarbonyliron lactone complexes in the synthesis of the resorcylic macrolides - and -zearalenol Steven V. Ley and Svenja Burckhardt pg 3028; DOI: 10.1039/b005942k |
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Functionalisation of 11C-labelled olefins via a Heck coupling reaction Margareta Björkman and Bengt Långström pg 3031; DOI: 10.1039/b003960h |
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Synthesis of annelated analogues of 6-benzyl-1-(ethoxymethyl)-5-isopropyluracil (MKC-442) using 1,3-oxazine-2,4(3H)-diones as key intermediates Janus S. Larsen Lene Christensen Gitte Ludvig Per T. Jørgensen Erik B. Pedersen and Claus Nielsen pg 3035; DOI: 10.1039/b005282p |
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Photochemical reactions of N-acylbenzoxazole-2-thiones Takehiko Nishio Ikuo Iida and Kunio Sugiyama pg 3039; DOI: 10.1039/b002548h |
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Asymmetric reduction of prochiral cycloalkenones. The influence of exocyclic alkene geometry Alison F. Simpson Corinna D. Bodkin Craig P. Butts Mark A. Armitage and Timothy Gallagher pg 3047; DOI: 10.1039/b004540n |
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Structural flexibility in the biocatalyst-mediated functionalization of ring A in salannin, a tetranortriterpene from Azadirachta indica K. Madhava Madyastha and Krishnamachari Venkatakrishnan pg 3055; DOI: 10.1039/b004260i |
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Reactions of diethyl azulene-1,3-dicarboxylate derivatives and 1-azaazulene derivatives with Grignard reagents, and alkyl- and aryllithium Tadayoshi Morita Noritaka Abe and Kahei Takase pg 3063; DOI: 10.1039/b003078n |
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Syntheses of three metabolites of icosapentaenoic and docosahexaenoic acids Solveig Flock and Lars Skattebøl pg 3071; DOI: 10.1039/b004101g |
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Synthesis and DNA-binding properties of bisdiazoliumylporphyrins Daryono H. Tjahjono Tomoko Yamamoto Sumito Ichimoto Naoki Yoshioka and Hidenari Inoue pg 3077; DOI: 10.1039/b005491g |
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A new and efficient synthesis of 2,2-disubstituted-3,4-dihydro-2H-1-benzopyrans Jhillu S. Yadav Basi V. Subba Reddy and Syed R. Hashim pg 3082; DOI: 10.1039/b004683n |
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Synthesis of 4-azido-3-diazo-3H-pyrazolo[3,4-b]quinoline from 3-amino-4-hydrazino-1H-pyrazolo[3,4-b]quinoline Wolfgang Stadlbauer and Gerhard Hojas pg 3085; DOI: 10.1039/b004681g |
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Synthesis and DNA cleavage of 2-O-amino-linked metalloporphyrin–oligonucleotide conjugates Igor Dubey Geneviève Pratviel and Bernard Meunier pg 3088; DOI: 10.1039/b004431h |
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1-(3,4-Dihydro-4-oxoquinazolin-3-yl)aziridines (Q-substituted aziridines): ring-opening reactions with C–N bond cleavage and preparation of Q-free chirons Robert S. Atkinson Andrew P. Ayscough William T. Gattrell and Tony M. Raynham pg 3096; DOI: 10.1039/b004798h |
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Reactions of 5-(4-chloro-5H-1,2,3-dithiazol-5-ylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione with primary and secondary alkylamines Moon-Kook Jeon and Kyongtae Kim pg 3107; DOI: 10.1039/b003109g |
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Chlorin-based symmetrical and unsymmetrical dimers with amide linkages: effect of the substituents on photodynamic and photophysical properties Gang Zheng Mohammad Aoudia David Lee Michael A. Rodgers Kevin M. Smith Thomas J. Dougherty and Ravindra K. Pandey pg 3113; DOI: 10.1039/b003367g |
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Synthesis of 1,1,6,6-tetramethylphosphajulolidine Peter G. Edwards Stephen J. Paisey and Robert P. Tooze pg 3122; DOI: 10.1039/b004525j |
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Intramolecular Diels–Alder reactions of 1-phenylsulfonylalka-1,2,( James R. Bull Richard Gordon and Roger Hunter pg 3129; DOI: 10.1039/b005146m |
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Synthesis of acyclic - and -silyl sulfimides Elena N. Suslova Svetlana V.Kirpichenko Aleksandr I. Albanov and Bagrat A. Shainyan pg 3140; DOI: 10.1039/b004761i |
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1,4-Asymmetric reduction of -keto sulfoxides bearing the 2,4,6-triisopropylphenyl group Shuichi Nakamura Masayuki Kuroyanagi Yoshihiko Watanabe and Takeshi Toru pg 3143; DOI: 10.1039/b004782l |
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Investigation of the reaction of 2-bromo-1-naphthol with arylacetonitriles and LiTMP: facile synthesis of 3-arylmethyl-1-hydroxynaphthalene-2-carbonitriles Sagun Tandel Anlai Wang Hongming Zhang Pervaiz Yousuf and Edward R. Biehl pg 3149; DOI: 10.1039/b003935g |
Issue 19
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Perkin 1 Abstracts:Solid Phase Organic Synthesis Catherine McCusker Tanya Wildman Fiona McKerlie Jason Tierney and Bernard Wathey pg 19-vii; DOI: 10.1039/b006705i |
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Synthetic receptors James H. Hartley Tony D. James and Christopher J. Ward pg 3155; DOI: 10.1039/a909641h |
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A novel stereo-controlled nucleobase exchange process for the synthesis of 2-C-branched nucleosides Volker Fehring Mai Yee Chan Ian A. O Neil and Richard Cosstick pg 3185; DOI: 10.1039/b007099h |
Synthesis of  -lactones from 2-alkynyl epoxides and 4-alkynyl-1,3-dioxolan-2-ones by palladium catalysed carbonylation and conjugate nucleophilic additionJulian G. Knight Simon W. Ainge Carl A. Baxter Timothy P. Eastman and Simon J. Harwood pg 3188; DOI: 10.1039/b006927m |
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Enantiospecific total synthesis of both enantiomers of 2-thiocyanatoneopupukeanane from (R)-carvone A. Srikrishna and Santosh J. Gharpure pg 3191; DOI: 10.1039/b005943i |
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The stereoselective preparation of substituted pyrrolidines using titanium- and zirconium-mediated diene metallabicyclisation methodology: the total synthesis of (–)--kainic acid Andrew D. Campbell Tony M. Raynham and Richard J. K. Taylor pg 3194; DOI: 10.1039/b005853j |
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Asymmetric reduction of ketones by Geotrichum candidum in the presence of AmberliteTM XAD, a solid organic solvent Kaoru Nakamura Mikio Fujii and Yoshiteru Ida pg 3205; DOI: 10.1039/b005204n |
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A comparison of some pyrolysis reactions of benzotriazoles, benzisoxazolones and benzisothiazolones Wit K. Janowski Rolf H. Prager and Jason A. Smith pg 3212; DOI: 10.1039/b004825i |
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Synthesis of -hydroxy-,-difluoro--ketoesters via [3,3]sigmatropic rearrangements Michael J. Broadhurst Samantha J. Brown Jonathan M. Percy and Michael E. Prime pg 3217; DOI: 10.1039/b004766j |
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The synthesis and reactivity of optically pure amino acids bearing side-chain thioamides John M. Sanderson P. Singh Colin W. G. Fishwick and John B. C. Findlay pg 3227; DOI: 10.1039/b004688o |
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Atropisomeric benzamides and naphthamides as chiral auxiliaries Jonathan Clayden Madeleine Helliwell Catherine McCarthy and Neil Westlund pg 3232; DOI: 10.1039/b004682p |
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Synthesis, structure and comparative stability of -hydrazono, oximino methyl ether and imino boronates Richard J. Mears Helen E. Sailes John P. Watts and Andrew Whiting pg 3250; DOI: 10.1039/b004573j |
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A novel approach to the enantioselective formal synthesis of pumiliotoxin 251D Yike Ni Gang Zhao and Yu Ding pg 3264; DOI: 10.1039/b004450o |
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Catalytic cyclopropanation of electron deficient alkenes mediated by chiral and achiral sulfides: scope and limitations in reactions involving phenyldiazomethane and ethyl diazoacetate Varinder K. Aggarwal Helen W. Smith George Hynd Ray V. H. Jones Robin Fieldhouse and Sharon E. Spey pg 3267; DOI: 10.1039/b004367m |
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Elucidation of the catalytic mechanisms of the non-haem iron-dependent catechol dioxygenases: synthesis of carba-analogues for hydroperoxide reaction intermediates Christopher J. Winfield Zeyana Al-Mahrizy Michael Gravestock and Timothy D. H. Bugg pg 3277; DOI: 10.1039/b004265j |
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An efficient synthesis of ()-piliformic acid Sivaprakasam Mangaleswaran and Narshinha P. Argade pg 3290; DOI: 10.1039/b004115g |
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A new version of the reverse-Cope elimination initiated by the nucleophilic addition of allylamines to nitrones: a synthesis of vicinal diamines Michael B. Gravestock David W. Knight K. M. Abdul Malik and Steven R. Thornton pg 3292; DOI: 10.1039/b003959o |
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Novel methodology for the solid-phase synthesis of phosphinic peptides Jens Buchardt and Morten Meldal pg 3306; DOI: 10.1039/b003848m |
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Carbanionic displacement reactions at phosphorus. Part III. Cyanomethylphosphonate vs. cyanomethylenediphosphonate. Synthesis and solid-state structures Bogdan Iorga Louis Ricard and Philippe Savignac pg 3311; DOI: 10.1039/b003371p |
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Synthesis of -substituted alanines via Michael addition of nucleophiles to dehydroalanine derivatives Paula M. T. Ferreira Hernâni L. S. Maia Luís S. Monteiro Joana Sacramento and Joana Sebastião pg 3317; DOI: 10.1039/b003353g |
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Dihydroisoquinolinium salts: catalysts for asymmetric epoxidation Philip C. Bulman Page Gerasimos A. Rassias David Barros Donald Bethell and Mark B. Schilling pg 3325; DOI: 10.1039/b002156n |
Issue 20
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Perkin 1 Abstracts: Biocatalysis in Organic Synthesis Gideon Grogan Alexis Carstairs Ian Jackson Denise McIntyre Alan Watt Sabine Flitsch and Nicholas Turner pg 20-ix; DOI: 10.1039/b007583n |
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Perkin 1 Abstracts: Natural Product Synthesis Jaqueline E. Milne Marcel de Puit and Duncan McArthur pg 20-xv; DOI: 10.1039/b007693g |
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Catalytic applications of transition metals in organic synthesis Louise Haughton and Jonathan M. J. Williams pg 3335; DOI: 10.1039/a909866f |
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Palladium-catalyzed regioselective arylation of silyloxy compounds with triarylantimony diacetates Suk-Ku Kang Hyung-Chul Ryu and Young-Taek Hong pg 3350; DOI: 10.1039/b006431i |
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Regioselective SN2 opening of ,-ethylenic epoxides by RLi–BF3 combination Alexandre Alexakis Emmanuel Vrancken Pierre Mangeney and Fabrice Chemla pg 3352; DOI: 10.1039/b005472k |
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Effect of BF3Et2O reagent on the base-promoted rearrangements of epoxides attached to eight-membered rings Alexandre Alexakis Emmanuel Vrancken and Pierre Mangeney pg 3354; DOI: 10.1039/b005474g |
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Synthesis of novel donor–acceptor twins Andreas Schultz Sabine Laschat Andrew P. Abbott Martin Langner and Toby B. Reeve pg 3356; DOI: 10.1039/b006736i |
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Studies on the asymmetric reduction of -oximino methyl ether boronates: reagent control, double diastereocontrol and transmitted remote asymmetric induction Helen E. Sailes John P. Watts and Andrew Whiting pg 3362; DOI: 10.1039/b005837h |
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The unexpected formation of bicyclo[2.2.1]heptane derivatives by Lewis acid-catalyzed transannular double cyclization Vattoly J. Majo Shuichi Suzuki Masahiro Toyota and Masataka Ihara pg 3375; DOI: 10.1039/b005727o |
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Desymmetrisation of 4,4-disubstituted cyclohexanones by enzyme-catalysed resolution of their enol acetates Graham Allan Andrew J. Carnell Maria Luisa Escudero Hernandez and Alan Pettman pg 3382; DOI: 10.1039/b005466f |
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Preparation of the tricyclic ketopyrrole core of roseophilin by radical macrocyclisation and Paal–Knorr condensation Jeremy Robertson Richard J. D. Hatley and David J. Watkin pg 3389; DOI: 10.1039/b005351l |
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Synthesis and absolute stereochemistry assignment of enantiopure dihydrofuro- and dihydropyrano-quinoline alkaloids Derek R. Boyd Narain D. Sharma Stephen A. Barr Jonathan G. Carroll Donald Mackerracher and John F. Malone pg 3397; DOI: 10.1039/b005285j |
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Syntheses of isotopically labelled L--amino acids with an asymmetric centre at C-3 John R. Harding Rachael A. Hughes Nicholas M. Kelly Andrew Sutherland and Christine L. Wilis pg 3406; DOI: 10.1039/b005172l |
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Preparation, X-ray structures and unique redox reactions of novel 2,2-(2,2-dimethylpropane-1,3-diylidene)bis(1,3-benzodithiole)-type electron donors fused with a naphthalene ring Takanori Suzuki Tsuyoshi Yoshino Masakazu Ohkita and Takashi Tsuji pg 3417; DOI: 10.1039/b005078o |
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Synthesis of N-unsubstituted bis[1,2]dithiolo[1,4]thiazines and bis[1,2]dithiolopyrroles Lidia S. Konstantinova Natalia V. Obruchnikova Oleg A. Rakitin Charles W. Rees and Tomás Torroba pg 3421; DOI: 10.1039/b005068g |
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Aerobic epoxidation of alkenes using polymer-bound Mukaiyama catalysts Bastienne B. Wentzel Salla-M. Leinonen Stephen Thomson David C. Sherrington Martinus C. Feiters and Roeland J. M. Nolte pg 3428; DOI: 10.1039/b005066k |
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Selectivity in the cycloadditions of carbonyl ylides with glyoxylates: an approach to the zaragozic acids—squalestatins David M. Hodgson James M. Bailey Carolina Villalonga-Barber Michael G. B. Drew and Timothy Harrison pg 3432; DOI: 10.1039/b004870o |
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New heteroditopic, linked macrocyclic systems derived from selectively protected N2S2-, N3O2- and N4-donor macrocycles Jy D. Chartres Andrew M. Groth Leonard F. Lindoy Mark P. Lowe and George V. Meehan pg 3444; DOI: 10.1039/b004797j |
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Tetrahydro-1,3-oxazin-6-ones as templates for the stereoselective synthesis of -substituted L-aspartic acids Guillaume Burtin Pierre-Jean Corringer and Douglas W. Young pg 3451; DOI: 10.1039/b004772o |
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Synthesis of C2-symmetric analogues of 4-(pyrrolidino)pyridine: new chiral nucleophilic catalysts Alan C. Spivey Adrian Maddaford Tomasz Fekner Alison J. Redgrave and Christopher S. Frampton pg 3460; DOI: 10.1039/b004704j |
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A study of the stereochemical features of 5-endo-trig iodocyclisations of 2-alkenylcycloalkan-1-ols Jenny M. Barks Gordon G. Weingarten and David W. Knight pg 3469; DOI: 10.1039/b004684l |
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Total synthesis of (–)-eudistomins with an oxathiazepine ring. Part 1. Formation of the oxathiazepine ring system Masako Nakagawa Jin-Jun Liu Tohru Hino Akihiko Tsuruoka Naoyuki Harada Makoto Ariga and Yasunori Asada pg 3477; DOI: 10.1039/b004570p |
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Total synthesis of (–)-eudistomins with an oxathiazepine ring. Part 2. Synthesis of (–)-eudistomins C, E, F, K, and L Jin-Jun Liu Tohru Hino Akihiko Tsuruoka Naoki Harada and Masako Nakagawa pg 3487; DOI: 10.1039/b004424p |
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Syntheses and characterization of 5-substituted hydantoins and thiazolines—implications for crystal engineering of hydrogen bonded assemblies. Crystal structures of 5-(2-pyridylmethylene)hydantoin, 5-(2-pyridylmethylene)-2-thiohydantoin, 5-(2-pyridylmethylene)thiazolidine-2,4-dione, 5-(2-pyridylmethylene)rhodanine and 5-(2-pyridylmethylene)pseudothiohydantoin Mubarik M. Chowdhry D. Michael P. Mingos Andrew J. P. White and David J. Williams pg 3495; DOI: 10.1039/b004312p |
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Proposed tennis ball and basket- and -lid routes to C60: two relevant C45 compounds Robert J. Ferrier Steven G. Holden and Olga Gladkikh pg 3505; DOI: 10.1039/b004272m |
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Photochemical substitution of polyhalogenothiophene and halogenothiazole derivatives Maurizio D Auria Claudio Distefano Franco DOnofrio Giacomo Mauriello and Rocco Racioppi pg 3513; DOI: 10.1039/b004002i |
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The conversion of racemic terminal epoxides into either (+)- or (–)-diol - and -lactones Zhi-Yu Liu Jian-Xin Ji and Bo-Gang Li pg 3519; DOI: 10.1039/b003793l |
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Cascade radical cyclisations leading to steroid ring constructions. Regio- and stereo-chemical studies using ester- and fluoro-alkene substituted polyene acyl radical intermediates Haydn M. Boehm Sandeep Handa Gerald Pattenden Lee Roberts Alexander J. Blake and Wan-Sheung Li pg 3522; DOI: 10.1039/b002999h |
Issue 21
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Dr Peter OBrien pg 21-vii; DOI: 10.1039/b007422p |
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Perkin 1 Abstracts: Solid Phase Organic Synthesis Catherine McCusker Tanya Wildman Fiona McKerlie Jason Tierney and Bernard Wathey pg 21-ix; DOI: 10.1039/b008207o |
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Bicyclic nucleosides and conformational restriction of oligonucleotides Michael Meldgaard and Jesper Wengel pg 3539; DOI: 10.1039/b000114g |
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Chemoenzymatic approaches to the decahydro-as-indacene cores associated with the spinosyn class of insecticide Martin Banwell David Hockless Bevyn Jarrott Brian Kelly Andrew Knill Robert Longmore and Gregory Simpson pg 3555; DOI: 10.1039/b006759h |
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Selective and rapid oxidation of primary, allylic and benzylic alcohols to the corresponding carbonyl compounds with NaNO2–acetic anhydride under mild and solvent-free conditions Babasaheb P. Bandgar Vaibhav S. Sadavarte and Lavkumar S. Uppalla pg 3559; DOI: 10.1039/b001215g |
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Stereoisomeric pyrimidine nucleoside analogues based on the 1,3-dihydrobenzo[c]furan core David F. Ewing Nour-Eddine Fahmi Christophe Len Grahame Mackenzie and Alessandra Pranzo pg 3561; DOI: 10.1039/b006417n |
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New asymmetric routes to ajmaline and suaveoline indole alkaloids Patrick D. Bailey Keith M. Morgan David I. Smith and John M. Vernon pg 3566; DOI: 10.1039/b005694o |
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The total synthesis of (–)-suaveoline Patrick D. Bailey and Keith M. Morgan pg 3578; DOI: 10.1039/b005695m |
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Chemistry of pyrrolizinones. Part 1. Reactions of pyrrolizin-3-ones with electrophiles: synthesis of 3,8-didehydroheliotridin-5-one Hamish McNab and Craig Thornley pg 3584; DOI: 10.1039/b005620k |
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A novel approach to bis-isoxazolines using a latent form of cyclopentadienone Sanjivanjit K. Basra Michael G. B. Drew John Mann and Peter D. Kane pg 3592; DOI: 10.1039/b005520o |
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Synthesis of the necine base (–)-supinidine from (S)-glutamic acid Carole M. Boynton Alan T. Hewson and Douglas Mitchell pg 3599; DOI: 10.1039/b005516f |
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Synthesis of sugar-modified analogs of bredinin (mizoribine), a clinically useful immunosuppressant, by a novel photochemical imidazole ring-cleavage reaction as the key step Satoshi Shuto Kimiyo Haramuishi Masayoshi Fukuoka and Akira Matsuda pg 3603; DOI: 10.1039/b005510g |
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Synthesis and evaluation of anti-HIV-1 activity of 3-azido-3-deoxy-2-O,4-C-methylene-linked bicyclic thymine nucleosides Anne G. Olsen Vivek K. Rajwanshi Claus Nielsen and Jesper Wengel pg 3610; DOI: 10.1039/b005469k |
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Regioselective reaction of 5,15-disubstituted porphyrins with organolithium reagents—synthetic access to 5,10,15-trisubstituted porphyrins and directly meso-meso-linked bisporphyrins Mathias O. Senge and Xiangdong Feng pg 3615; DOI: 10.1039/b005411i |
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Regulation of diastereoselectivity through the epimerisation of a cyclic intermediate in the reaction of cyclic ketene ortho ester with aldehydes Chan-Mo Yu Jae-Young Lee Kwangwoo Chun Junhee Lee and Yong-Am Lee pg 3622; DOI: 10.1039/b005086p |
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Selective conjugate addition to zerumbone and transannular cyclization of its derivatives Kouichi Ohe Koji Miki Shin-ichi Yanagi Takumi Tanaka Seiji Sawada and Sakae Uemura pg 3627; DOI: 10.1039/b004284f |
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Considerations on the stereoselective synthesis of dibrominated spiro-1,3-dioxanes. Synthesis and stereochemistry of monobrominated precursors Elena Bogdan Ion Grosu Eugen Mesaros Loïc Toupet Gerard Plé Sorin Mager and Luminita Muntean pg 3635; DOI: 10.1039/b004282j |
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Direct thioalkylation of nitroquinolines with alkanethiolate anions via nucleophilic displacement of a ring hydrogen atom Takehiko Kawakami and Hitomi Suzuki pg 3640; DOI: 10.1039/b004190o |
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Parallel solution-phase syntheses of functionalised bicyclo[2.2.2]octanes: generation of a library using orchestrated multi-step sequences of polymer-supported reagents and sequesterants Steven V. Ley and Alessandro Massi pg 3645; DOI: 10.1039/b003129l |
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Tetrahydrofuran amino acids—versatile building blocks for unnatural biopolymers: lack of secondary structure in oligomeric carbopeptoids derived from a D-galacto-5-(aminomethyl) tetrahydrofuran-2-carboxylic acid Dominic E. A. Brittain Mark P. Watterson Timothy D. W. Claridge Martin D. Smith and George W. J. Fleet pg 3655; DOI: 10.1039/b002995p |
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Tetrahydrofuran amino acids: Secondary structure in tetrameric and octameric carbopeptoids derived from a D-allo 5-(aminomethyl)tetrahydrofuran-2-carboxylic acid Natasha L. Hungerford Timothy D. W. Claridge Mark P. Watterson Robin T. Aplin Andres Moreno and George W. J. Fleet pg 3666; DOI: 10.1039/b002996n |
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Tetrahydrofuran amino acids: - and -azidotetrahydrofurancarboxylic acid monomers derived from D-glucoheptonolactone as building blocks for - and -oligopeptides Natasha L. Hungerford and George W. J. Fleet pg 3680; DOI: 10.1039/b002997l |
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Heterocyclic sulfones. Part IV. A novel synthesis of pyrrole and fused heterocyclic sulfones Ayman Wahba Erian Yvette Abd El-sayed Issac Sherif Mourad Sherif and Fivian Farouk Mahmoud pg 3686; DOI: 10.1039/b002494p |
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New reductive addition of hard nucleophiles to 6,7-bis(methylsulfanyl)-1,4-dihydro-1,4-methanonaphthalene-5,8-dione Claudio Di Vitta Ivan P. de Arruda Campos João P. S. Farah and Júlio Zukerman-Schpector pg 3692; DOI: 10.1039/b000575o |
Issue 22
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Professor Patrick D. Bailey Patrick D. Bailey pg 22-ix; DOI: 10.1039/b001667p |
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Perkin 1 Abstracts: Biocatalysis in Organic Synthesis Gideon Grogan Alexis Carstairs Ian Jackson Denise McIntyre Alan Watt Sabine Flitsch and Nicholas Turner pg 22-xi; DOI: 10.1039/b008425p |
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Perkin 1 Abstracts: Natural Product Synthesis Jacqueline E. Milne Marcel de Puit and Duncan McArthur pg 22-xviii; DOI: 10.1039/b008605n |
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Nitro and related compounds Joseph P. Adams and Jody R. Paterson pg 3695; DOI: 10.1039/a901139k |
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Tricyclic nucleosides derived from D-glucose. Synthesis and conformational behaviour Poul Nielsen Michael Petersen and Jens Peter Jacobsen pg 3706; DOI: 10.1039/b006082h |
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Synthesis based on cyclohexadienes. Part 34. A tandem cationic rearrangement–ene cyclisation route to 2-pupukeanone P. John Biju Krishna Kaliappan M. S. Laxmisha and G. S. R. Subba Rao pg 3714; DOI: 10.1039/b003409f |
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A facile access to the synthesis of functionalised unsymmetrical biaryls from 2H-pyran-2-ones through carbanion induced C–C bond formation Vishnu J. Ram Mahendra Nath Pratibha Srivastava Sanjay Sarkhel and Prakas R. Maulik pg 3719; DOI: 10.1039/b005572g |
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Stereoselective reduction of chiral 2-furoic acid derivatives using group I metals in ammonia Timothy J. Donohoe Andrew A. Calabrese Clare A. Stevenson and Tamara Ladduwahetty pg 3724; DOI: 10.1039/b006390h |
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Synthesis of C-ring substituted xanthones from the [4+2] cycloaddition reaction of vinylchromones and acyclic enamines Avijit S. Kelkar Roy M. Letcher Kung-Kai Cheung Kwei-Fung Chiu and Geoffrey D. Brown pg 3732; DOI: 10.1039/b004422i |
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Nitrilimine cycloadditions in aqueous media Giorgio Molteni Marco Orlandi and Gianluigi Broggini pg 3742; DOI: 10.1039/b005567k |
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NIR chromophores from small acetylenic building blocks: a Diels–Alder approach to octaalkynylphthalocyanines Rüdiger Faust and Frieder Mitzel pg 3746; DOI: 10.1039/b006114j |
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New derivatives of the 1,2-benzodiazepine ring system David W. Knight and Paul B. Little pg 3752; DOI: 10.1039/b005696k |
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Bakers yeast-mediated enantioselective synthesis of the bisabolane sesquiterpenes (+)-curcuphenol, (+)-xanthorrhizol, (–)-curcuquinone and (+)-curcuhydroquinone Claudio Fuganti and Stefano Serra pg 3758; DOI: 10.1039/b006141g |
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Chemoselective debenzylation of N-benzyl tertiary amines with ceric ammonium nitrate Steven D. Bull Stephen G. Davies Garry Fenton Andrew W. Mulvaney R. Shyam Prasad and Andrew D. Smith pg 3765; DOI: 10.1039/b006852g |
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Synthesis and reactivity of pentavalent biphenyl-2,2-ylenebismuth derivatives Alexey Yu. Fedorov and Jean-Pierre Finet pg 3775; DOI: 10.1039/b006307j |
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Selectivity enhancement of epoxide hydrolase catalyzed resolution of 2,2-disubstituted oxiranes by substrate modification Ingrid Osprian Wolfgang Stampfer and Kurt Faber pg 3779; DOI: 10.1039/b005203p |
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A versatile and efficient method for the synthesis of benz[a]azulenic enones starting from readily available o-(2-furyl)cycloheptatrienylbenzenes Misako Sasabe Yuuko Houda Hideki Takagi Takashi Sugane Xu Bo and Kimiaki Yamamura pg 3786; DOI: 10.1039/b005948j |
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Zinc bromide as catalyst for the stereoselective construction of quaternary carbon: improved synthesis of diastereomerically enriched spirocyclic diols Yong Qiang Tu Chun An Fan Shi Kuo Ren and Albert S. C. Chan pg 3791; DOI: 10.1039/b006182o |
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Cycloaddition reactions of 2-oxo-2H-cyclohepta[b]furan derivatives with arylacetylenes and the di--methane rearrangement of homobarrelene derivatives Vijay Nair Mecheril Valsan Nandakumar Gopinathan Nair Anilkumar Davis Maliakal Mariappanadar Vairamani Sripadi Prabhakar and Nigam P. Rath pg 3795; DOI: 10.1039/b005377p |
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Palladium-catalyzed intermolecular carboazidation of allenes with aryl iodides and trimethylsilyl azide Hao-Ming Chang and Chien-Hong Cheng pg 3799; DOI: 10.1039/b004524l |
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Palladium catalysed cross-coupling of (fluoroarene)tricarbonylchromium(0) complexes René Wilhelm and David A. Widdowson pg 3808; DOI: 10.1039/b006576p |
Issue 23
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Multi-step organic synthesis using solid-supported reagents and scavengers: a new paradigm in chemical library generation Steven V. Ley Ian R. Baxendale Robert N. Bream Philip S. Jackson Andrew G. Leach Deborah A. Longbottom Marcella Nesi James S. Scott R. Ian Storer and Stephen J. Taylor pg 3815; DOI: 10.1039/b006588i |
Issue 24
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Dr Neil S. Isaacs Dr Neil S. Isaacs pg 24-xvii; DOI: 10.1039/b008420o |
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Perkin 1 Abstracts: Solid Phase Organic Synthesis Catherine McCusker Tanya Wildman Fiona McKerlie Jason Tierney and Bernard Wathey pg 24-xxvii; DOI: 10.1039/b008837o |
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Perkin 1 Abstracts: Natural Product Synthesis Jaqueline E. Milne Marcel de Puit and Duncan McArthur pg 24-xxxvii; DOI: 10.1039/b009147m |
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Perkin 1 Abstracts: Solid Phase Organic Synthesis Gideon Grogan Alexis Carstairs Ian Jackson Denise McIntyre Alan Watt Sabine Flitsch and Nicholas Turner pg 24-xxxiii; DOI: 10.1039/b009353j |
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Applications of aliphatic unsaturated non-proteinogenic -H--amino acids Floris P. J. T. Rutjes Larissa B. Wolf and Hans E. Schoemaker pg 4197; DOI: 10.1039/b001538p |
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Supported catalysts and their applications in synthetic organic chemistry Yolanda R. de Miguel pg 4213; DOI: 10.1039/a906850c |
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Synthesis of the novel amine (R*,R*,R*)-tris(-methylbenzyl)amine. X-Ray crystal structures of racemic and enantiomerically pure forms Paul Wyatt Craig P. Butts Vipulkumar Patel and Ben Voysey pg 4222; DOI: 10.1039/b007710k |
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Synthesis of highly functionalised, optically active disaccharide receptors by sequential aryl–alkyne cross- and oxidative acetylenic homo-coupling Anne Sophie Droz and François Diederich pg 4224; DOI: 10.1039/b007706m |
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Highly stereoselective total synthesis of PM-Toxin B, a corn host-specific pathotoxin Mitsuru Hosaka Hiroyuki Hayakawa and Masaaki Miyashita pg 4227; DOI: 10.1039/b007617l |
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Synthesis of dendritic iron(II) porphyrins with a tethered axial imidazole ligand designed as new model compounds for globins Philipp Weyermann and François Diederich pg 4231; DOI: 10.1039/b007611m |
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Application of the Ugi four-component condensation reaction for the synthesis of ,- and ,-dipeptides substituted with fluoroarylalkyl pendent groups Norio Shibata Biplab Kumar Das and Yoshio Takeuchi pg 4234; DOI: 10.1039/b007455l |
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One pot synthesis of a chiral N-phosphine substituted iminophosphorane: X-ray structure and in situ NMR study Andrei S. Batsanov Matthew G. Davidson Ignacio Fernández Judith A. K. Howard Fernando López-Ortiz and Richard D. Price pg 4237; DOI: 10.1039/b005816p |
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A new and facile stereocontrolled synthesis of conjugated dienyl trifluoromethyl ketones Jingbo Xiao Yanshu Feng and Chengye Yuan pg 4240; DOI: 10.1039/b005250g |
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Chemistry of L-ascorbic acid. Part 3. Photoreduction of quinones with 5,6-O-isopropylidene-L-ascorbic acid Mukund G. Kulkarni and Sandesh D. Kate pg 4242; DOI: 10.1039/b005120i |
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Reaction of magnesiated bases on substituted pyridines: deprotonation or 1,4-addition? Véronique Bonnet Florence Mongin François Trécourt and Guy Quéguiner pg 4245; DOI: 10.1039/b007270m |
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First enantioselective total synthesis of (natural) (+)-11,12-epoxy-11,12-dihydrocembrene-C and (–)-7,8-epoxy-7,8-dihydrocembrene-C Zuosheng Liu Weidong Z. Li Lizeng Peng Ying Li and Yulin Li pg 4250; DOI: 10.1039/b007239g |
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HYDRA: A novel hydroxy and amine functionalised resin synthesised by reductive amination of PEG aldehyde and a polyamine Thomas Groth Morten Grøtli William D. Lubell Les P. Miranda and Morten Meldal pg 4258; DOI: 10.1039/b007141m |
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Synthesis of the farnesyl ether 2,3,5-trifluoro-6-hydroxy-4-[(E,E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yloxy]nitrobenzene, and related compounds containing a substituted hydroxytrifluorophenyl residue: novel inhibitors of protein farnesyltransferase, geranylgeranyltransferase I and squalene synthase Jonathan H. Marriott Amelia M. Moreno Barber Ian R. Hardcastle Martin G. Rowlands Rachel M. Grimshaw Stephen Neidle and Michael Jarman pg 4265; DOI: 10.1039/b007101n |
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Chemical and electro-chemical reduction of qinghaosu (artemisinin) Wen-Min Wu and Yu-Lin Wu pg 4279; DOI: 10.1039/b007056o |
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A new route to hydrophobic amino acids using copper-promoted reactions of serine-derived organozinc reagents Hervé J. C. Deboves Urszula Grabowska Adriana Rizzo and Richard F. W. Jackson pg 4284; DOI: 10.1039/b007032g |
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Enantiomerically pure cyclopropylboronic esters: auxiliary- versus substrate-control Jörg Pietruszka and Andreas Witt pg 4293; DOI: 10.1039/b006970l |
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Palladium(II)-catalysed oxidation of alcohols under an oxygen atmosphere in a fluorous biphase system (FBS) Takahiro Nishimura Yasunari Maeda Nobuyuki Kakiuchi and Sakae Uemura pg 4301; DOI: 10.1039/b006874h |
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Oxidative cyclisation of N,N-dialkylcatechol amines to heterocyclic betaines via o-quinones: synthetic, pulse radiolytic and enzyme studies John Clews Christopher J. Cooksey Peter J. Garratt Edward J. Land Christopher A. Ramsden and Patrick A. Riley pg 4306; DOI: 10.1039/b006860h |
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On the coupling of aryldiazonium salts with N,N-disubstituted 2-aminothiophenes and some of their carbocyclic and heterocyclic analogues Horst Hartmann and Ines Zug pg 4316; DOI: 10.1039/b006803i |
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Stereoselective construction of vicinal stereogenic quaternary carbon atoms. Enantiospecific approaches to (+)-valerane Adusumilli Srikrishna Ranganathan Viswajanani and Chikkana Dinesh pg 4321; DOI: 10.1039/b006757l |
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(Fluoren-9-ylmethoxy)carbonyl (Fmoc) amino acid azides: Synthesis, isolation, characterisation, stability and application to synthesis of peptides Vommina V. Suresh Babu Kuppanna Ananda and Ganga-Ramu Vasanthakumar pg 4328; DOI: 10.1039/b006756n |
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Trivinylogs of Crystal Violet: synthesis and absorption properties of new near-IR dyes Saumitra Sengupta and Subir Kumar Sadhukhan pg 4332; DOI: 10.1039/b006693l |
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A new synthesis of aryl isothiocyanates: carbon disulfide as a dipolarophile. The reaction of (4,5,6,7-tetrahydro-2H-1,2,3-benzotriazolium-1-yl)arylaminide 1,3-dipoles with carbon disulfide: synthesis, kinetics, mechanism. Azolium 1,3-dipoles Richard N. Butler and Leonie M. Wallace pg 4335; DOI: 10.1039/b006631l |
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Total syntheses of three natural products, vignafuran, 2-(4-hydroxy-2-methoxyphenyl)-6-methoxybenzofuran-3-carboxylic acid methyl ester, and coumestrol from a common starting material Kou Hiroya Naoyuki Suzuki Akito Yasuhara Yuya Egawa Atsushi Kasano and Takao Sakamoto pg 4339; DOI: 10.1039/b006623k |
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Synthesis and structures of pyrroles fused with rigid bicyclic ring systems at -positions Hidemitsu Uno Satoshi Ito Mitsuo Wada Hikaru Watanabe Miho Nagai Akiko Hayashi Takashi Murashima and Noboru Ono pg 4347; DOI: 10.1039/b006584f |
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Cycloadditions of 1-aza-2-azoniaallene ions to alkenes Wolfgang G. Wirschun Yaseen A. Al-Soud Konstanze A. Nusser Olli Orama Gerd-Michael Maier and Johannes C. Jochims pg 4356; DOI: 10.1039/b006525k |
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Stereochemical and mechanistic features of asymmetric Pauson–Khand processes Alan R. Kennedy William J. Kerr David M. Lindsay James S. Scott and Stephen P. Watson pg 4366; DOI: 10.1039/b006523o |
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Synthesis of tricyclic -lactams related to cephalosporins Nigel K. Capps Gareth M. Davies David Loakes and Douglas W. Young pg 4373; DOI: 10.1039/b006415g |
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Synthesis and reactions of Biginelli-compounds. Part 23. Chemoenzymatic syntheses of enantiomerically pure 4-aryl-3,4-dihydropyrimidin-2(1H)-ones Barbara Schnell Wolfram Krenn Kurt Faber and C. Oliver Kappe pg 4382; DOI: 10.1039/b006372j |
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The biosynthesis of pramanicin in Stagonospora sp. ATCC 74235: a modified acyltetramic acid Paul H. M. Harrison Petar A. Duspara Stephen I. Jenkins Salima A. Kassam David K. Liscombe and Donald W. Hughes pg 4390; DOI: 10.1039/b006007k |
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Synthesis and investigation of the configurational stability of some dimethylammonium borate salts Stuart Green Adam Nelson Stuart Warriner and Benjamin Whittaker pg 4403; DOI: 10.1039/b005954o |
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New potential (P,S)-ligands containing tetrathiafulvalene Pascal Pellon Emilie Brulé Nathalie Bellec Karine Chamountin and Dominque Lorcy pg 4409; DOI: 10.1039/b005835l |
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Stereoisomerism in 3-[N-(2-acetoxypropanoyl)-N-acylamino]quinazolin-4(3H)-ones, enantioselective acylating agents Abdullah G. Al-Sehemi Robert S. Atkinson John Fawcett and David R. Russell pg 4413; DOI: 10.1039/b005814i |
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Efficient routes to alkyl ether linked derivatives of 1,1-(bi-2-naphthol) bearing 3-N,N-dialkylamide substituents Anthony Cunningham Michael R. Dennis and Simon Woodward pg 4422; DOI: 10.1039/b005701k |
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Organic chemistry of enyne sulfones: convenient one-pot synthesis of 2-ethoxy-3-ethynyl-4-methylene-2-perfluoroalkyl-3-(phenylsulfonyl)tetrahydrofurans Mitsuhiro Yoshimatsu and Junichi Murase pg 4427; DOI: 10.1039/b005698g |
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Antitumour imidazotetrazines. Part 39. Synthesis of bis(imidazotetrazine)s with saturated spacer groups Jill Arrowsmith Sharon A. Jennings David A. F. Langnel Richard T. Wheelhouse and Malcolm F. G. Stevens pg 4432; DOI: 10.1039/b005652i |
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The importance of ester and alkoxy type functionalities for the chemo- and enantio-recognition of substrates by hydrolysis with Candida rugosa lipase Francesca Bellezza Antonio Cipiciani Gabriele Cruciani and Francesco Fringuelli pg 4439; DOI: 10.1039/b005512n |
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Bi-imidazole nucleosides obtained by ring opening of etheno and substituted etheno derivatives of adenosine Jukka Mäki Rainer Sjöholm and Leif Kronberg pg 4445; DOI: 10.1039/b005407k |
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One-pot transformation of cyclic phosphine oxides to phosphine–boranes by dimethyl sulfide–borane György Keglevich Melinda Fekete Tungalag Chuluunbaatar András Dobó Veronika Harmat and László Tke pg 4451; DOI: 10.1039/b005380p |
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The scope and limitation of the [1,4]-SPh shift in the synthesis of allylic alcohols Varinder K. Aggarwal Jason Eames Maria A. de las Heras Sara McIntyre and Stuart Warren pg 4456; DOI: 10.1039/b005349j |
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Indium-mediated reductive dehalogenation of -halocarbonyl compounds in water Leeyoung Park Gyochang Keum Soon Bang Kang Kwan Soo Kim and Youseung Kim pg 4462; DOI: 10.1039/b005278g |
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Diastereoselective intramolecular [4+4] photocycloaddition reaction of N-(naphthylcarbonyl)anthracene-9-carboxamides: temperature effects and reversal of diastereoselectivity Shigeo Kohmoto Hyuma Masu Chuya Tatsuno Keiki Kishikawa Makoto Yamamoto and Kentaro Yamaguchi pg 4464; DOI: 10.1039/b005142j |
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Synthesis of cyclopentenones and butenolides by reaction of the lithium salt of P,P-diphenyl-P-(alkyl)(N-phenyl)phosphazenes with electrophilic double and triple bonds Julia M. Álvarez-Gutiérrez Fernando López-Ortiz Santiago García-Granda and Alejandra Rodríguez-González pg 4469; DOI: 10.1039/b005131o |
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Cycloaddition-mediated strategies for synthesis of perhydrobenzo[14,15]-14-19-norsteroids James R. Bull and Eugene S. Sickle pg 4476; DOI: 10.1039/b005129m |
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Intramolecular functionalisation by a methylene radical of a 1,2-diol and a vicinal amino alcohol: models for coenzyme B12-dependent diol dehydratase and ethanolamine ammonia lyase Rosaleen J. Anderson Susan Ashwell Ian Garnett and Bernard T. Golding pg 4488; DOI: 10.1039/b004917o |
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A simple preparation of syn-NH-amide aldols and amide-Baylis–Hillman adducts via a Michael–aldol tandem process Akio Kamimura Yoji Omata Hiromasa Mitsudera and Akikazu Kakehi pg 4499; DOI: 10.1039/b004721j |
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Combining high pressure and catalysis: pinacol- or catecholborane hydroboration of functionalized olefins Sylvie Colin Lucile Vaysse-Ludot Jean-Pierre Lecouvé and Jacques Maddaluno pg 4505; DOI: 10.1039/b004275g |
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Synthesis based on cyclohexadienes. Part 35: Synthesis of some polyquinane derivatives P. John Biju M. S. Laxmisha and G. S. R. Subba Rao pg 4512; DOI: 10.1039/b003548n |
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Alkylation and addition to isocyanate of 2-(5-amino-3,4-dicyano-2H-pyrrol-2-ylidene)-1,1,2-tricyanoethanide. X-Ray crystal and molecular structures of methyl-, dimethyl-, dimethylaminoethylene- and propylaminocarbonyl-amino derivatives Vincenzo Fares Alberto Flamini and Pamela Pasetto pg 4520; DOI: 10.1039/b003407j |